Table 2.
Sample a | % of Starting Material (w/w) | Mn (Da) | Mw (Da) | Đ |
---|---|---|---|---|
K-LF-0 | - | 1600 | 4260 | 2.7 |
K-LFa-R5 b | 72 | n.a. | n.a. | n.a. |
K-LFa-R2 | 4.8 | 1060 | 2000 | 1.9 |
K-LFa-P2 | 2.5 | 575 | 840 | 1.5 |
K-LFo-R5 | 7.9 | 740 | 1320 | 1.8 |
K-LFo-R2 | 1.7 | 530 | 860 | 1.6 |
K-LFo-P2 | 1.1 | 480 | 740 | 1.5 |
a Samples were eluted after acetylation. The reported values for molecular weights are relative to polystyrene standards. b This fraction was found to be poorly soluble in the eluting solvent (THF) even after acetylation, preventing the possibility of performing GPC analysis.