Table 1.
NMR spectral data of mucoroidiol (1) a.
| 13C | (DEPT) | 1H | |
|---|---|---|---|
| 1 | 37.0 | CH2 | 1.23 (1H, dd, J = 12.5, 6.5 Hz) |
| 1.32–1.37 (1H, m) | |||
| 2 | 45.6 | CH | 1.84 (1H, dt, J = 12.9, 6.5 Hz) |
| 3 | 39.0 | C | |
| 4 | 31.7 | CH2 | 1.42–1.47 (1H, m) |
| 2.03 (1H, q, J = 9.4 Hz) | |||
| 5 | 24.4 | CH2 | 1.33–1.37 (1H, m) |
| 2.14–2.21 (1H, m) | |||
| 6 | 40.2 | CH | 1.33–1.39 (1H, m) |
| 7 | 44.7 | CH | 1.60–1.63 (1H, m) |
| 8 | 30.3 | CH2 | 0.78 (1H, q, J = 12.9 Hz) |
| 1.35–1.41 (1H, m) | |||
| 9 | 38.4 | CH | 2.10–2.16 (1H, m) |
| 10 | 42.8 | CH2 | 1.30–1.35 (1H, m) |
| 1.59 (1H, dd, J = 13.5, 7.8 Hz) | |||
| 11 | 41.7 | C | |
| 12 | 73.0 | CH2 | 3.34 (1H, d, J = 10.6 Hz) |
| 3.37 (1H, d, J = 10.6 Hz) | |||
| 13 | 26.5 | CH3 | 0.99 (3H, s) |
| 14 | 67.2 | CH2 | 3.32–3.37 (1H, m) |
| 3.51 (1H, dd, J = 10.5, 4.8 Hz) | |||
| 15 | 26.3 | CH3 | 1.11 (3H, s) |
a 600 MHz for 1H and 150 MHz for 13C in CDCl3.