Table 2.
δC | δH (J in Hz) | HMBC (H→C) Correlations | |
---|---|---|---|
1 | 136.2 | - | |
2 | 113.8 | - | |
3 | 130.5 | - | |
4 | 126.6 | 7.67, s | C-1, C-2, C-4, C-4a, C-8a, C-9, C-10 |
4a | 133.6 | - | |
5 | 112.4 | 7.34, s | C-4, C-8a, C-6, C-7 |
6 | 151.3 | - | |
7 | 150.2 | - | |
8 | 111.5 | 8.30, s | C-1, C-4a, C-6, C-7 |
8a | 124.5 | - | |
9 | 172.1 | ||
10 | 162.4 | - | |
1′ | 111.5 | - | |
2′ | 144.0 | - | |
3′ | 104.5 | 6.91, s | C-1, C-1′, C-2′, C-4′, C-5′ |
4′ | 149.6 | - | |
5′ | 147.1 | - | |
6′ | 113.8 | 8.02, s | C-1, C-1, C-2′, C-4′, C-5′ |
1″ | 62.8 | 4.43, q (7.0) | C-9, C-2″ |
2″ | 14.2 | 1.41, t (7.0) | C-1″ |