. Author manuscript; available in PMC: 2020 Jul 24.

Published in final edited form as: Biochim Biophys Acta. 2011 Nov 27;1824(3):422–432. doi: 10.1016/j.bbapap.2011.10.017

Table 3.

Summary of refinement statistics.

Crystal form	Orthorhombic	Monoclinic

Resolution range (Å)	39.84 – 1.97	72.74 – 1.55
R_work (%)	17.2	15.9
R_free (%)	21.6	19.4
Number of protein atoms	3303	3438
Number of water molecules	451	699
RMSD bond length (Å)	0.014	0.015
RMSD bond angles (°)	1.401	1.524
Ramachandran Plot Statistics
Most favored regions (%)	95.52	96.84
Additional allowed regions (%)	2.59	2.92

R_work = Σ_hkl ||F_obs(hkl)| - |F_calc(hkl)||/ Σ_hkl |F_obs|, R_free is calculated with 5% of total number of reflections.