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. 2020 Jun 8;26(37):8281–8285. doi: 10.1002/chem.202000134

Figure 3.

Figure 3

A) Progress of the gram‐scale synthetic/biocatalytic production of 1 from 2, as verified by UHPLC and HR‐ESIMS analyses of an aliquot. Top trace: overlaid individual chromatograms of authentic 1 and 2. B) 3D plot of UHPLC diode array and total ion chromatogram (TIC) data of the singly chromatographed 1 production assay. TIC trace a) ESI (+); trace b) ESI (−) mode.