Table 2.
Textural properties of synthesized nanostructures.
| Sample | SBET (m2 g−1)a | PV (cm3 g−1)b | PVmicro (cm3 g−1)c | PR (Å)d | ρ (g cm−3)e | dS (nm)f | dXRD (nm)g | Acid amount (mmol g−1)h |
|---|---|---|---|---|---|---|---|---|
| C1 | 19 | 0.08 | – | 80 | 1.3 | 243 | 5.7 | 0.25 |
| C2 | 17 | 0.09 | – | 97 | 1.3 | 271 | 9.5 | 0.4 |
| C3 | 29 | 0.15 | 0.001 | 106 | 1.5 | 137 | n. d. | 0.06 |
| C4 | 51 | 0.31 | 0.004 | 127 | 1.3 | 90 | 4.5 | 0.05 |
| GO | 11 | 0.08 | – | 119 | 0.8 | 681 | 32 | 0.49 |
| C1g | 59 | 0.09 | 0.008 | 46 | 1.2 | 84 | 4.9 | 0.26 |
| C4g | 111 | 0.17 | 0.02 | 67 | 1.3 | 41 | 4.4 | 0.43 |
Surface area determined by BET method based on N2 adsorption.
BJH adsorption cumulative volume of pores with radius of 8.5–1,500 Å.
t-plot micropore volume.
Pore radius, BJH method on N2 adsorption.
Bulk density.
Crystallite size based on BET surface area: dS = 6 / (SBET·ρ), ρ bulk density (Hiyoshi, 2012).
Diameter of product particle measured by XRD according to Scherrer's equation (Alhassan et al., 2015): using 222 diffraction of yttrium oxide phase.
Determined by n-butylamine titration.