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. 2020 Jul 17;76(Pt 8):1311–1315. doi: 10.1107/S2056989020009512
O1—C1 1.1943 (18) O1A—C1A 1.1913 (17)
O2—C2 1.1904 (17) O2A—C2A 1.1871 (18)
O3—C1 1.3868 (17) O3A—C1A 1.3855 (17)
O3—C2 1.3978 (16) O3A—C2A 1.3905 (18)
C1—C3 1.5014 (18) C1A—C3A 1.5048 (18)
C2—C4 1.5024 (18) C2A—C4A 1.5080 (19)
C3—H3 1.0000 C3A—H3A 1.0000
C3—C4 1.5360 (17) C3A—C4A 1.5409 (17)
C3—C8 1.5596 (18) C3A—C8A 1.5607 (17)
C4—H4 1.0000 C4A—H4A 1.0000
C4—C5 1.5631 (17) C4A—C5A 1.5616 (18)
C5—H5 1.0000 C5A—H5A 1.0000
C5—C6 1.5040 (19) C5A—C6A 1.5068 (19)
C5—C10 1.5321 (19) C5A—C10A 1.5326 (19)
C6—H6 0.9500 C6A—H6A 0.9500
C6—C7 1.329 (2) C6A—C7A 1.3312 (19)
C7—H7 0.9500 C7A—H7A 0.9500
C7—C8 1.504 (2) C7A—C8A 1.5028 (18)
C8—H8 1.0000 C8A—H8A 1.0000
C8—C9 1.5337 (19) C8A—C9A 1.5313 (19)
C9—H9 1.0000 C9A—H9A 1.0000
C9—C10 1.5110 (19) C9A—C10A 1.5131 (18)
C9—C11 1.5066 (19) C9A—C11A 1.5091 (19)
C10—H10 1.0000 C10A—H10A 1.0000
C10—C11 1.500 (2) C10A—C11A 1.507 (2)
C11—H11C 0.9900 C11A—H11A 0.9900
C11—H11D 0.9900 C11A—H11B 0.9900
C1—O3—C2 110.55 (11) C1A—O3A—C2A 110.90 (11)
O1—C1—O3 119.75 (13) O1A—C1A—O3A 119.95 (13)
O1—C1—C3 129.86 (13) O1A—C1A—C3A 129.73 (13)
O3—C1—C3 110.39 (11) O3A—C1A—C3A 110.31 (11)
O2—C2—O3 119.55 (13) O2A—C2A—O3A 120.26 (14)
O2—C2—C4 130.45 (13) O2A—C2A—C4A 129.74 (14)
O3—C2—C4 110.00 (11) O3A—C2A—C4A 109.97 (11)
C1—C3—H3 110.1 C1A—C3A—H3A 110.6
C1—C3—C4 104.49 (10) C1A—C3A—C4A 104.31 (11)
C1—C3—C8 112.48 (11) C1A—C3A—C8A 111.28 (11)
C4—C3—H3 110.1 C4A—C3A—H3A 110.6
C4—C3—C8 109.58 (10) C4A—C3A—C8A 109.43 (10)
C8—C3—H3 110.1 C8A—C3A—H3A 110.6
C2—C4—C3 104.53 (10) C2A—C4A—C3A 104.27 (11)
C2—C4—H4 110.0 C2A—C4A—H4A 110.7
C2—C4—C5 112.25 (11) C2A—C4A—C5A 110.36 (11)
C3—C4—H4 110.0 C3A—C4A—H4A 110.7
C3—C4—C5 109.95 (10) C3A—C4A—C5A 109.80 (10)
C5—C4—H4 110.0 C5A—C4A—H4A 110.7
C4—C5—H5 111.9 C4A—C5A—H5A 111.8
C6—C5—C4 106.76 (11) C6A—C5A—C4A 105.79 (10)
C6—C5—H5 111.9 C6A—C5A—H5A 111.8
C6—C5—C10 110.54 (12) C6A—C5A—C10A 110.44 (11)
C10—C5—C4 103.44 (10) C10A—C5A—C4A 104.84 (10)
C10—C5—H5 111.9 C10A—C5A—H5A 111.8
C5—C6—H6 122.6 C5A—C6A—H6A 122.6
C7—C6—C5 114.75 (12) C7A—C6A—C5A 114.74 (12)
C7—C6—H6 122.6 C7A—C6A—H6A 122.6
C6—C7—H7 122.6 C6A—C7A—H7A 122.6
C6—C7—C8 114.89 (12) C6A—C7A—C8A 114.71 (12)
C8—C7—H7 122.6 C8A—C7A—H7A 122.6
C3—C8—H8 111.8 C3A—C8A—H8A 111.7
C7—C8—C3 107.11 (11) C7A—C8A—C3A 106.74 (10)
C7—C8—H8 111.8 C7A—C8A—H8A 111.7
C7—C8—C9 110.60 (11) C7A—C8A—C9A 110.65 (11)
C9—C8—C3 103.41 (10) C9A—C8A—C3A 104.13 (10)
C9—C8—H8 111.8 C9A—C8A—H8A 111.7
C8—C9—H9 117.1 C8A—C9A—H9A 116.9
C10—C9—C8 110.50 (11) C10A—C9A—C8A 110.59 (11)
C10—C9—H9 117.1 C10A—C9A—H9A 116.9
C11—C9—C8 121.54 (12) C11A—C9A—C8A 122.06 (12)
C11—C9—H9 117.1 C11A—C9A—H9A 116.9
C11—C9—C10 59.62 (9) C11A—C9A—C10A 59.82 (9)
C5—C10—H10 116.9 C5A—C10A—H10A 117.1
C9—C10—C5 110.79 (11) C9A—C10A—C5A 110.56 (11)
C9—C10—H10 116.9 C9A—C10A—H10A 117.1
C11—C10—C5 121.90 (12) C11A—C10A—C5A 121.31 (12)
C11—C10—C9 60.05 (9) C11A—C10A—C9A 59.96 (9)
C11—C10—H10 116.9 C11A—C10A—H10A 117.1
C9—C11—H11C 117.7 C9A—C11A—H11A 117.7
C9—C11—H11D 117.7 C9A—C11A—H11B 117.7
C10—C11—C9 60.33 (9) C10A—C11A—C9A 60.22 (9)
C10—C11—H11C 117.7 C10A—C11A—H11A 117.7
C10—C11—H11D 117.7 C10A—C11A—H11B 117.7
H11C—C11—H11D 114.9 H11A—C11A—H11B 114.9