Bruker APEXII CCD diffractometer | 2441 reflections with I > 2σ(I) |
φ and ω scans | Rint = 0.039 |
Absorption correction: multi-scan (SADABS; Bruker, 2013) | θmax = 70.2°, θmin = 4.0° |
Tmin = 0.578, Tmax = 0.753 | h = −15→15 |
23789 measured reflections | k = −7→7 |
2683 independent reflections | l = −21→21 |