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. Author manuscript; available in PMC: 2021 Jul 1.
Published in final edited form as: J Am Chem Soc. 2020 Jun 23;142(26):11388–11393. doi: 10.1021/jacs.0c05362

Figure 2.

Figure 2.

(A) Synthesis and crystal structure of [(BPhen)CuII(N3)(μ-N3)]2 (hydrogen atoms and chlorobenzene molecule omitted for clarity). (B) Reaction of [(BPhen)CuII(N3)(μ-N3)]2 with Gomberg’s dimer (6 mol% Cu(OAc)2/BPhen, 3.6 equiv. TMSN3, 2.5 equiv. NFSI).