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. 2020 Jul 21;5(30):18675–18684. doi: 10.1021/acsomega.0c01405

Table 3. DSC Data and Crystallinity Obtained by Wide-Angle X-Ray Diffraction (WAXD) Characterization for PLA/OMMT Composites with Different OMMT and EGDE Contents.

samples Tg (°C) Tcc (°C) Tm1 (°C) Tm2 (°C) ΔHcc (J/g) ΔHm (J/g) χc-DSC (%) χc-WAXD (%)
neat PLA 58.9 112.8 163.1 170.8 23.67 24.81 1.23 0.73
PLA/OMMT-2 58.4 108.8 163.5 169.8 23.70 25.76 2.26 1.85
PLA/OMMT-4 59.1 110.0 163.2 169.6 24.12 26.87 3.08 2.72
PLA/OMMT-6 58.7 109.2 162.8 169.7 24.52 27.24 3.11 2.93
PLA/OMMT-8 58.8 111.4 163.4 169.7 24.15 26.55 2.80 2.82
PLA/OMMT-10 59.2 112.7 164.2 170.0 23.24 25.84 3.10 2.90
PLA/EGDE1/OMMT-6 56.2 106.4   168.4 24.53 28.76 4.83 3.95
PLA/EGDE2/OMMT-6 55.0 104.1   167.7 24.25 32.52 9.45 11.87
PLA/EGDE4/OMMT-6 56.5 107.1   169.0 25.84 34.83 10.28 22.75
PLA/EGDE6/OMMT-6 56.2 104.0   167.9 23.96 30.92 7.95 0.71