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. 2020 Jul 11;10(20):8996–9031. doi: 10.7150/thno.45413

Table 6.

Potential toxicity of AgNPs in vivo and in vitro

Objects Exposure Toxicity References
Animal model In vitro/vivo Cell lines/Tissues Size; Shape Dosages Route Time Effect Toxicity manners
Pig In vitro and vivo HEKs and porcine skin 20, 50 and 80 nm 0.34, 1.7 μg/mL Incubation; skin contact Acute: 18 and 24 h;
chronic: 14 d
Focal inflammation Dose-dependent 350
Mice In vivo Liver Less than 30 nm 10 ppm Skin contact 2, 7 and 14 d Central venous dilation; hyperemia, cell swelling, Kupffer and inflammatory cells increase Time-dependent 332
Mice In vivo Spleen, liver, lung and kidney 12-20 nm 7.5, 30 and 120 mg/kg Intravenous administration 7 and 14 d Induction of inflammatory reactions in lung and liver cells Gender-, concentration- and time-dependent 346
Mice In vivo Lung 10-20 nm; spherical 10, 100, 1000 and 10,000 ppm Intratracheally administration 1, 3, 7 and 15 d Acute lung inflammation and bronchitis; hyperplasia of alveolar epithelial cells Dose-dependent 330
Mice In vivo Liver, spleen, kidneys, heart, lungs, testes, stomach, intestine and seminal vesicles 3±1.57 nm; spherical 11.4-13.3 mg/kg Intravenous injection 1, 28 d Inflammatory response; alteration of hematological factors; change of gene expression; ROS generation Dose-dependent 351
Mice In vivo Liver, kidneys and lung 10, 75 and 110 nm; spherical 25 μg/mice Intravenous administration 1, 3 and 7 d Peripheral inflammation in liver, kidneys and lungs Time-, concentration- and size-dependent 343
Mice In vivo Lung 20 and 110 nm 0.05, 0.15, 0.45 and 1.35 mg/kg Intratracheal instillation 1, 7 and 21 d Alter SP-D level; deficit immune defense function Size- and stabilization-dependent 44
Mice In vivo Brain, lung, liver, kidney and testis 22, 42 and 71 nm 0.25 mg/kg, 0.50 mg/kg, 1.00 mg/kg Oral administration 14 and 28 d Induce organ toxicity and inflammatory responses Dose-dependent 352
Mice In vivo heart, lung, kidney, liver and blood 1.4-250nm 11.4-13.3mg/kg body weight Intravenous administration 28 d Induce gene expression; ROS generation; apoptosis Dose-dependent 351
Mice In vitro and in vivo A549, BxPC-3; PC-3; Hep G2, CNE; AsPC-1; U-87 MG; SW480; EC109; MDA-MB-231; VSMC; HMEC; LO2; 293FT; tumor, brain, heart, kidney, lung, spleen, and liver 19.2±3.8 Ång, spherical or ellipsoidal 0-32ng/µl, 1.875 mg/kg Intravenous administration Acute: 24 h; chronic: 28 d None Dose- and time-dependent 21
Mice in vivo Lung 20 and 110 nm, spherical 0.1, 0.5 and 1.0 mg/kg Inhalation Acute: 40 h; chronic: 21 d Pulmonary fibrosis Size- and coating-dependent 353
Mice in vivo Kidney, liver and spleen 2.45-19.53 nm 0.37, 0.65, 13 and 21 mg/kg Oral administration 27 d Tissue destruction; cell necrosis and apoptosis dose-dependent 354
Rat In vivo Brain >100 nm 5 and 50 mg/kg Oral administration 79 d Cell death, disturbed neurotransmitter and cytokine production, ROS generation -- 355
Rat In vivo Sperm and testicular tissue 60-80 nm 30, 125 and 300 mg/kg Intraperitoneal injection 28 d Decrease normal sperm morphology, sperm vitality and sperm count Dose-dependent 348
Rat In vivo Kidneys, liver and blood 20-65 nm 2,000 mg/kg Intraperitoneal administration 3 d Liver and kidney damage Time- and dose-dependent 356
Rat In vivo Lung, spleen, liver, kidney, thymus and heart 6.3-629 nm 0.5 mg/kg Intravenous administration 24 h Liver and kidney damage; chromosome breakage; genotoxicity Dose-dependent 357
Rat In vivo Epididymal sperm 20-30 nm 50, 100 and 200 mg/kg Oral administration 90 d Sperm anomalies; decrease sperm viability Dose-dependent 37
Rat In vivo Brain 3-10 nm, spherical 1 and 10 mg/kg Intragastric administration 14 d Neuron shrinkage; cytoplasmic or foot swelling of astrocytes Dose-dependent 38
Rats In vivo Kidney, liver and blood 20-60 nm, spherical 2,000 mg/kg bw, twice injections Intraperitoneal injection 5 d Liver and kidney damage; blood parameters disrupt Dose- and time-dependent 356
Rat In vivo Spleen, liver, and lymph nodes and blood 20 nm and 100 nm 6 mg/kg Intravenous administration 28 d Suppression of the natural killer cell activity; stimulate LPS mitogen; increase cytokine production Dose-dependent 358
Rat In vivo Liver and kidney 56 nm 30, 125 and 500 mg/kg Oral administration 90 d Liver damage; bile-duct hyperplasia Dose- and gender-dependent 341
Rat In vivo Kidney 52.7-70.9 nm 10 ml/kg Oral administration 90 d Deposite in kidneys Dose-dependent 340
Female ICR mice; male guinea pigs In vivo Oral, skin and eye 10-20 nm, spherical 5,000 mg/kg (oral);
50 and 5,000 ppm (eye);
50 and 100,000 ppm (skin)
Oral administration;
eye drops;
skin contact
1, 2 and 3 day Conjunctivae irritation 326
Male ICR mice In vivo Blood, liver, spleen, kidney, lungs and brain 10, 40 and 100 nm, spherical 10 mg/kg Intravenous injection 24 h Bleeding or necrosis of multiple internal organs Size- and tissue-dependent 331
BN and SD rats In vivo Lung 20, 110 nm, spherical 0.1 mg/kg or 90 breaths/minute Intratracheal administration 1, 7 and 21 d Lung eosinophilia and bronchial hyperresponsiveness; distruction of blood/alveolar epithelial permeability barrier Dose- and size-dependent; rat strains related 46
Mice and guinea pigs in vivo Lung, lymph node, heart, liver and kidney 10-20 nm, spherical 5,000 mg/kg, 5000 ppm Oral administration, eye and skin contact 14 d No mortality and toxic signs 326
Freshwater fish In vivo Embryo 25.9-36.7 nm, spherical Acute: 0.3, 0.6, 1.2, 2.4 and 4.8 mg/L; subchronic: 0.05, 0.1, 0.25 and 0.5 mg/L Incubation 14 d Liver damage; deplete glutathione; deactivate lactate dehydrogenase and antioxidant enzymes Time- and dose-dependent 39
Japanese medaka in vivo Embryo 20-37 nm, spherical 0, 0.5, 1.0, 2.0, 4.0 and 8.0 mg/L Oral administration 48 h death dose-dependent 327
Zebrafish In vivo Embryo 20 and 110 nm, spherical 0.08, 0.4, 2, 1,0 and 50 mg/L Hatch 5 d Multiple developmental abnormalities Size- and surface coating-dependent 359
Zebrafifish In vitro and in vivo Brain, heart, yolk and blood of embryo 5-20 nm 5, 10, 25, 50 and 100 µg/mL Hatch 24, 48 and 72 h Multiple developmental abnormalities Concentration-dependent 43
Drosophila melanogaster in vivo Parents, egg and offspring 2-20 nm 10, 20, 30, 40, 50 and 100 mg/L Oral administration 5,10, 15, 30, 45, 60 and 95 min Abdominal pigmentation Dose-dependent 360
Drosophila melanogaster In vivo Germline stem cell; testis 20 nm 2, 3.5 and 5 mg/L Oral administration 24h, 5 d Delay the development of the F1 offsprings; ROS generation; premature GSC differentiation Dose-dependent 42
Caenorhabditis elegans In vivo The worms' body 96.4±35.6 nm, spherical 0-1mg/L Culture 6 and 24 h DNA damage, ROS generation, inhibition of growth Dose- and time-dependent 361
Caenorhabditis elegans In vitro The worms' body < 100 nm, spherical 0.025, 0.05 and 0.075 µg/mL Culture 24 h ROS generation; DNA damage Size-dependent 152
In vitro rat brain microvascular endothelial cells, pericytes, and astrocytes 7±2 nm 1 and 10 μg/mL Incubation 24 h Trx system, Nr4a1 and Dusp1 regulaion , inflammation and apoptosis Dose-dependent 338
In vitro Mouse ESCs 20.2 ±4.1 nm, spherical 5.0 µg/ml 24 h Heat shock protein and the metallothionein families regulation, induce oxidative stress and apoptosis Dose-dependent 362
In vitro Mouse microglia N9 cell line, N27 neuronal cells 49.7±10.5 nm, spherical 50 μg/mL Incubation 24 h Nitric oxide and TNFα production Dose-dependent 363
In vitro Mouse lymphoma cell line, human lymphoblastoid cells 20, 50 and 100 nm, spherical 0-400 μg/mL Incubation 4, 8, and 24 h DNA mutants Size-, concentration- and coating-dependent 47
In vitro Rat primary cerebral astrocytes 24.18±4.14 nm, spherical 0.01, 0.1, 1 and 10 mg/mL Incubation 24 h Neuroinflammation and apoptosis; increase caspase activities Dose-dependent 337
In vitro Primary astrocyte cell, rat glioma C6 cell line 6.9-8.7 nm, spherical 0.1, 1, 10, 50, 75 and 100 µg/mL Incubation 24 h Necrosis and apoptosis Dose-dependent 364
In vitro Murine brain ALT astrocytes, murine microglial BV-2 cells and mouse neuroblastoma Neuro-2a (N2a) cells 3-5 nm 0.5, 1, 5, 10 and 12.5µg/mL Incubation 24 h Cytokine secretion, Aβ amyloid deposition, inflflammatory response Dose-dependent 339
In vitro UMR-106 6 nm, cubic 10, 25, 50, 100, 150 and 225 μM Incubation 24h Decrease lysosomal and mitochondrial activity Dose-dependent 365
In vitro U937 cell 4,20 and 70 nm, round 1.56, 3.12, 6.25, 12.5, 25 and 50 µg/mL Incubation 24 h Oxidative stress; cytokines release Size-dependent 50
In vitro HepG2 cell line 20 nm 2.5 to 50 µg/cm3 Incubation 24 h Endogenous antioxidant defence regulation Dose-dependent 366
In vitro Jurkat T, NCI-H460, HeLa cells, HepG2, MCF-7, Beas-2B 5-10 nm 0.2, 0.5 and 1 mg/L Incubation 4, 12 and 24 h DNA damage; p38 MAPK activation; cell arrest; apoptosis Time- and concentration- dependent 27
In vivo Human lymphocytes and sperms 8-10 nm Density gradient: 1:9, 1:3, 1:1 30 and 60 mins Cell viability decrease Concentration- and time-dependent 367
In vitro Pk15 61.2±33.9 nm, nonuniform 50 mg/L Incubation 24 and 48 h Genotoxicity in Pk15 cells Dose-dependent 342
In vitro Zebrafish ovarian follicle cells 30-55 nm 30 μg/mL Incubation 2 h Apoptosis of ovarian follicle cells; germinal vesicle breakdown Concentration-dependent 349

*NOTE: UMR 106, rat osteosarcoma cells; MDA-MB-231, triple negative breast cancer cell line; PMBC, peripheral blood mononuclear cell; HepG2, human liver cancer cell line; Jurkat T, human T lymphocyte cell line; NCI-H460, human lung cancer cell line; MCF-7, human breast cancer cell line; Beas-2B: human bronchial epithelial cells; SPD, surfactant protein-D; U937, human histiocytic lymphoma cell line; Pk15, pig kidney cell line; BV-2, murine microglial cell line; N2a cells, mouse neuroblastoma; HEKs, human embryonic kidney cells; A549, human lung carcinoma; BxPC-3, human pancreas adenocarcinoma cells; PC3, prostate adenocarcinoma cells; HepG2, hepatocellular carcinoma cells; ESCs, embryonic stem cell; CNE, nasopharyngeal carcinoma cells; AsPC-1, pancreas adenocarcinoma cells; U-87 MG, glioblastoma cells; SW480, colorectal adenocarcinoma cells; EC109, esophageal cancer cells; VSMC, vascular smooth muscle cells; HMEC, human microvascular endothelial cells; LO2, hepatocytes; 293FT, embryonic kidney cells.