Table 2.
Summary of crystallographic statistics.
| FjGH20 | FjChiB | |
|---|---|---|
| Data collection | ||
| Date | April 14, 2016 | May 3, 2017 |
| Source | BL 14.1 at Bessy | ID30A-3 at ESRF |
| Wavelength (Å) | 0.918409 | 0.9677 |
| Space group | P 21 21 21 | P 1 21 1 |
| Cell dimensions | ||
| a, b, c (Å) | 75.99, 124.55, 151.59 | 43.91, 66.44, 53.44 |
| α, β, γ (°) | 90, 90, 90 | 90, 98.31, 90 |
| No. of measured reflections | 1,033,044 (35,652) | 163,627 (14,163) |
| No. of independent reflections | 158,136 (7,637) | 34,484 (2,962) |
| Resolution (Å) | 49.1–1.7 (1.73–1.70) | 36.4–1.6 (1.69–1.63) |
| Rmerge (%) | 7.10 (39.4) | 4.30 (20.7) |
| CC1/2 (%) | 99.9 (86.8) | 99.8 (98.0) |
| Mean I/σI | 17.2 (3.2) | 19.7 (6.3) |
| Completeness (%) | 99.9 (98.4) | 90.7 (77.9) |
| Redundancy | 6.5 (4.7) | 4.8 (4.7) |
| Refinement | ||
| Rwork/Rfree | 0.142/0.175 | 0.157/0.189 |
| No. atoms | ||
| Protein | 10,214 | 2,523 |
| Ligand/ions | 22 | 15 |
| Water | 1544 | 338 |
| B-factors | ||
| Protein | 14.7 | 23.2 |
| Water | 23.9 | 34.2 |
| RMSD | ||
| Bond length (Å) | 0.020 | 0.006 |
| Bond angles (°) | 1.95 | 0.77 |
| PDB accession | 6YHH | 6XYZ |