Table 4.
Solvent | Product with methanol | t1/2 with MeOH (min) | t1/2 without MeOH (min) | |
---|---|---|---|---|
Glucoside (%) | Orthoester (%) | |||
Et2O | 40 | 1 | 15 | >1000 |
THF | 0 | 50 | 70 | 70 |
EtOAc | 10 | 10 | 10 | 25 |
CH2Cl2 | 30 | 10 | 15 | 50 |
acetone | 5 | 30 | 10 | 15 |
Solvent | Product with methanol | t1/2 with MeOH (min) | t1/2 without MeOH (min) | |
---|---|---|---|---|
Glucoside (%) | Orthoester (%) | |||
Et2O | 40 | 1 | 15 | >1000 |
THF | 0 | 50 | 70 | 70 |
EtOAc | 10 | 10 | 10 | 25 |
CH2Cl2 | 30 | 10 | 15 | 50 |
acetone | 5 | 30 | 10 | 15 |