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Experimental Setting of thermogravimetric and differential scanning calorimetry.
| TGA | DSC | ||
|---|---|---|---|
| Instrument: | Perkin Elmer Pyrus 7 TGA | Instrument: | TA Q2000 DSC |
| Sample Size: | ~3.0 mg | Sample Size: | ~3.0 mg |
| Sample Pan: | Standard Aluminum Pan | Sample Pan: | Aluminum |
| Temperature Range: | 30–800 C | Temperature Range: | 90–180 C |
| Scanning Rate: | 10–50 °C/min | Rate of Heating or Cooling: | 10 °C/min |
| Purge Gas and Rate: | N2 at 20 mL/min | Purge Gas and Rate: | N2 at 20 mL/min |
