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(a) Scheme for the preparation of cell lysate samples. (b) Representative SAMDI-MS spectra of untreated (left) and isocitrate/NADP+-treated (right) lysates displaying 12C αKG capture at m/z = 1091 (sodium adduct of α-cleavage product), 13C αKG capture at m/z = 1095 (sodium adduct of α-cleavage product) and pyruvate capture at m/z = 1099 (sodium adduct).
