Table 1.
Statistics for the X‐ray data collection for the new OXA‐10_IPM, OXA‐10_ETP and OXA‐655_MEM structures.
| OXA‐10_IPM | OXA‐10_ETP | OXA‐655_MEM | |
|---|---|---|---|
| Diffraction source | BESSY BL14.1 | BESSY BL14.1 | BESSY BL14.1 |
| Wavelength (Å) | 0.9184 | 0.9184 | 0.9184 |
| Temperature (K) | 100 | 100 | 100 |
| Detector | Pilatus 6M | Pilatus 6M | Pilatus 6M |
| Crystal‐detector distance (mm) | 371.15 | 207.79 | 282.96 |
| Rotation range per image (°) | 0.1 | 0.1 | 0.1 |
| Total rotation range (°) | 130 | 200 | 200 |
| Space group | P212121 | P212121 | P21 |
| a, b, c (Å) | 94.93 | 48.39 | 68.14 |
| 124.79 | 94.78 | 82.44 | |
| 48.48 | 125.59 | 99.00 | |
| α, β, γ (°) | 90 90 90 | 90 90 90 | 90 97.01 90 |
| Resolution range (Å) | 45.0–1.89 (1.96–1.89) | 25.0–1.85 (1.89–1.85) | 25–2.10 (2.15–2.10) |
| Total no. of reflections | 580 336 (51 160) | 370 553 (19 418) | 242 812 (17 796) |
| No. of unique reflections | 46 526 (4266) | 50 164 (3035) | 61 827 (4483) |
| Completeness (%) | 99.0 (92.4) | 99.9 (99.8) | 94.9 (92.9) |
| Redundancy | 4.8 (4.9) | 7.4 (6.4) | 5.8 (1.4) |
| 〈I/σ(I)〉 | 12.3 (1.1) | 8.5 (1.0) | 5.8 (1.5) |
| R meas. | 0.1675 (1.731) | 0.168 (1.705) | 0.184 (0.824) |
| CC 1/2 | 0.997 (0.553) | 0.996 (0.420) | 0.979 (0.539) |
| Overall B‐factor from Wilson plot (Å2) | 28.6 | 20.8 | 15.7 |