Table 2.
OXA‐10_IPM | OXA‐10_ETP | OXA‐655_MEM | |
---|---|---|---|
PDB entry | 6SKP | 6SKR | 6SKQ |
Resolution range (Å) | 45.0–1.89 (1.96–1.89) | 25.0–1.85 (1.92–1.85) | 25.0–2.10 (2.18–2.10) |
No. of reflections, working set | 46 466 (4265) | 50 073 (4900) | 61 782 (6070) |
No. of reflections, test set | 2099 (192) | 2482 (263) | 2426 (233) |
Final R cryst | 0.2188 (0.3228) | 0.1757 (0.3031) | 0.1770 (0.2390) |
Final R free | 0.2511 (0.3458) | 0.2253 (0.3309) | 0.2319 (0.2875) |
No. of protein chains/Tot. no of residues | 2/491 | 2/490 | 4/980 |
R.m.s.d | |||
Bonds (Å) | 0.013 | 0.010 | 0.003 |
Angles (°) | 1.21 | 1.09 | 0.59 |
Average B factors (Å2) | 39.02 | 36.68 | 21.34 |
Protein | 39.0 | 36.0 | 20.44 |
Chain A/B/C/D | 33.2/43.5 | 25.6/46.3 | 19.4/20.2/21.3/19.9 |
Solvent | 46.3 | 40.7 | 28.67 |
Ramachandran plot | |||
Favoured/Allowed/outliers (%) | 96.5/3.3/0.2 | 96.9/3.1/0.0 | 96.5/3.2/0.3 |
Clashscore | 8.09 | 7.44 | 3.10 |