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. 2020 Aug 6;25(16):3571. doi: 10.3390/molecules25163571

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© 2020 by the authors.

Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).

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Solid-State NMR (ssNMR) spectra with magic angle spinning (MAS) of ⍺-syn oligomers. (A) ¹³C-¹³C dipolar-assisted rotational resonance (DARR) correlation spectra showing the aliphatic regions of type A (left) and type B (right) oligomers; (B) Insensitive nuclei enhanced by polarization transfer (INEPT) correlation spectra. The regions of the spectra that were detected are assigned with the respective residue number and highlighted in green in the bars on top. The labels ca, cb, cg, cd, and ce represent C^⍺, C^β, C^γ, C^δ, and C^ℇ atoms, respectively. Reprinted with permission from The American Association for the Advancement of Science. Science 2017, 358, 1440–1443. Copyright © 2017, Copyright © 2017 The Authors, some rights reserved; exclusive licensee American Association for the Advancement of Science.