Table 3.
Entry | Time (h) | V H2O (mL) | Urea Amount (mol) | Observations |
---|---|---|---|---|
1 | 120 | 360 | 0.485 | Well-dispersed spheres of 260(26) nm; NC size (PXRD): 20.2(2) nm. |
2 | 120 | 720 | 0.485 | Well-dispersed spheres of 233(41) nm; NC size (PXRD): 21.8(3) nm. |
3 | 120 | 200 | 0.485 | Well-dispersed spheres of 229(20) nm; NC size (PXRD): 25.2(4) nm. |
4 | 120 | 360 | 0.166 | Very well-dispersed spheres of 338(35) nm; NC size (PXRD): 26.9(3) nm. |
5 | 120 | 360 | 1.415 | Agglomerated spheres of 75(34) nm; NC size (PXRD): 22.2(2) nm. |
6 | 120 | 360 | 0.832 | Well-dispersed spheres of 219(24) nm; NC size (PXRD): 21.2(2) nm. |
7 | 120 | 200 | 0.832 | Very well-dispersed spheres of 155(20) nm; NC size (PXRD): 30(5) nm. |