Skip to main content
. 2020 Jun 12;59(13):8916–8924. doi: 10.1021/acs.inorgchem.0c00734

Figure 4.

Figure 4

Room-temperature solid-state CP-MAS 31P NMR spectra of the adduct [PS3Bi]2[BOT], PS3BiI3, PS3BiBr3, and PS3BiCl3 (at spinning rates of 8, 6, 6, and 10 kHz, respectively). For an easier comparison of the band widths, the resonances of [PS3Bi]2[BOT] and PS3BiX3 (X = I, Br, Cl)52 have been centered at the same position. For all samples the line widths of the bands have been proven to be independent from the applied spinning rates. The symbols * and # indicate spinning side bands and [HPS3]+[OTf]− impurity, respectively.