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Reagents and conditions: (a) (i) PMe3, THF, then H2O; (ii) appropriate RCOOH, EDC, CH2Cl2; (b) H2, Pd black; (c) (i) PMe3, THF, then H2O; (ii) (Boc)2O, Et3N, CH2Cl2; (d) (i) HCl, AcOH, H2O; (ii) nervonic acid, oxalyl chloride, reflux; the acyl chloride is added to crude amine in THF/aq. NaOAc.
