Bruker Kappa Mach3 APEXII diffractometer	2784 independent reflections
Radiation source: 0.2 × 2 mm2 focus rotating anode	2699 reflections with I > 2σ(I)
MONTEL graded multilayer optics monochromator	Rint = 0.041
Detector resolution: 66.67 pixels mm-1	θmax = 72.2°, θmin = 4.9°
φ– and ω–scans	h = −21→22
Absorption correction: gaussian (SADABS; Krause et al., 2015)	k = −9→9
Tmin = 0.297, Tmax = 0.586	l = −24→24
49954 measured reflections