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. 2020 Jul 13;295(36):12635–12647. doi: 10.1074/jbc.RA120.014534

Table 2.

Crystallographic data collection and refinement statistics

Statistics for the highest-resolution shell are shown in parentheses.

P-Rex 1 DEP1 domain
Wavelength 1.033
Resolution range 19.49-3.12 (3.23-3.12)
Space group P6322
Unit cell (Å, ˚) 103 103 70.0 90 90 120
Total reflections 34,606
Unique reflections 4,064 (379)
Multiplicity 19 (1.3)
Completeness (%) 98.5 (94.5)
Mean I/σ(I) 19 (1.3)
Wilson B-factor 97.7
Rmeas 0.15 (0.60)
Rpim 0.05 (0.32)
CC1/2 1 (0.71)
Reflections used in refinement 4,061 (379)
Reflections used for R-free 213 (20)
Rwork 0.228 (0.343)
Rfree 0.254 (0.386)
Number of nonhydrogen atoms 754
    Solvent atoms 4
    Protein residues 91
Root mean square (distances) 0.013
Root mean square (angles) 2.10
Ramachandran favored (%) 91.0
Ramachandran allowed (%) 6.70
Ramachandran outliers (%) 2.30
Rotamer outliers (%) 8.6
Clash score 15.9
Average B-factor 79.1
    Macromolecule 79.3
    Solvent 45.0
Number of TLS groups 1