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. Author manuscript; available in PMC: 2020 Sep 15.
Published in final edited form as: Methods Mol Biol. 2018;1777:23–68. doi: 10.1007/978-1-4939-7811-3_2

Table 2:

Typical parameters for a 1H-13C cross-polarization experiment.

MAS rate: 25 kHz (rotor period, τr = 40 μs)
Pulse Power
(kHz)
Duration (μs) Phase
pH,1(π/2) 110 2.27 y,−y
pH,2 Linear ramp: 50 to 100 2,000 x
pC,1 50 2000 x,x,y,y,−x,−x,−y,−y
pC,2 0* 5 y,y,−x,−x,−y,−y,x,x
ϕReceiver x,−x,y,−y,−x,x,−y,y
Delay Duration
d1 2 s
Decoupling
period
Power (kHz) Method
dec1 100 TPPM
comments *zero except during calibration