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. Author manuscript; available in PMC: 2020 Sep 15.
Published in final edited form as: Methods Mol Biol. 2018;1777:23–68. doi: 10.1007/978-1-4939-7811-3_2

Table 3:

Typical parameters for calibration of frequency selective pulse.

MAS rate: 10 kHz (rotor period, τr = 100 μs)
Pulse Power
(kHz)
Duration (μs) Phase
pH,1(π/2) 110 2.27 (x)8, (−x)8
pH,2 Linear Ramp between 40 to 80 2000 y
pC,1 50 2000 y
pC,2 (π/2) 50 5 x,−x
pC,3 (π, Gaussian) 0.5* 1000 x
pC,4 (π/2) 50 5 x,x,y,y,−x,−x,−y,−y
ϕReceiver x,−x,y,−y,−x,x,−y,y,−x,x,−y,y,x,−x,y,−y
Delay Duration
d1 2 s
Decoupling period Power (kHz) Method
dec1 110 TPPM
comments *The power designated for the Gaussian pulse is the average power.