Table 4:
Typical parameters for 2D-fpRFDR experiment.
MAS rate: 25 kHz (rotor period, τr = 40 μs) | |||
---|---|---|---|
Pulse | Power (kHz) |
Duration (μs) |
Phase |
pH,1 | 110 | 2.27 | (x)8, (−x)8 |
pH,2 | Linear ramp between 50 and 100 | 2,000 | y |
pC,1 | 50 | 2,000 | y |
pC,2 (π/2) | 50 | 5 | x,−x and y,−y for each t1 |
pC,3 (π)* | 37.5 | x,y,x,y,y,x,y,x,−x,−y,−x,−y,−y,−x,−y,−x | |
pC,4 (π/2) | 50 | 5 | x,x,y,y,−x,−x,−y,−y |
ϕReceiver | x,−x,y,−y,−x,x,−y,y,−x,x,−y,y,x,−x,y,−y | ||
Delay | Duration (s) | ||
d1 | 2 | ||
t1 | varied for 2D acquisition | ||
Decoupling period |
Power (kHz) | Method | |
dec1 | 110 | Two-pulse phase modulation (TPPM) | |
comments | N = 32 |