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. Author manuscript; available in PMC: 2020 Sep 15.
Published in final edited form as: Methods Mol Biol. 2018;1777:23–68. doi: 10.1007/978-1-4939-7811-3_2

Table 4:

Typical parameters for 2D-fpRFDR experiment.

MAS rate: 25 kHz (rotor period, τr = 40 μs)
Pulse Power
(kHz)
Duration
(μs)
Phase
pH,1 110 2.27 (x)8, (−x)8
pH,2 Linear ramp between 50 and 100 2,000 y
pC,1 50 2,000 y
pC,2 (π/2) 50 5 x,−x and y,−y for each t1
pC,3 (π)* 37.5 τr3=13.33 x,y,x,y,y,x,y,x,−x,−y,−x,−y,−y,−x,−y,−x
pC,4 (π/2) 50 5 x,x,y,y,−x,−x,−y,−y
ϕReceiver x,−x,y,−y,−x,x,−y,y,−x,x,−y,y,x,−x,y,−y
Delay Duration (s)
d1 2
t1 varied for 2D acquisition
Decoupling
period
Power (kHz) Method
dec1 110 Two-pulse phase modulation (TPPM)
comments N = 32