Table 8:
Typical parameters for REDOR experiment.
| MAS rate: 10 kHz (rotor period, τr = 100 μs) | |||
|---|---|---|---|
| Pulse | Power (kHz) |
Duration (μs) | Phase |
| pH,1(π/2) | 110 | 2.27 | y,−y |
| pH,2 | Linear ramp: 40 to 80 | 2,000 | x |
| pC,1 | 50 | 2,000 | x,x,y,y,−x,−x,−y,−y |
| pC,2 (π) | 50 | 10 | x,x,y,y,−x,−x,−y,−y |
| pN,1 (π) | 50 | 10 | x,y |
| ϕReceiver | x,−x,y,−y,−x,x,−y,y | ||
| Delay | Duration | ||
| d1 | 2 s | ||
| Decoupling period | Power (kHz) | Method |
|---|---|---|
| dec1 | 110 | CW |
| dec2 | 110 | TPPM |
| comments | Loop parameter N: 1, 2, 3,… | |
| The experiment is run as a pseudo-2D sequence, where instead of t1 the loop parameter n is increased from 1 to 2, 3… | ||