. Author manuscript; available in PMC: 2021 Mar 8.

Published in final edited form as: Nat Struct Mol Biol. 2020 Sep 8;27(9):863–869. doi: 10.1038/s41594-020-0489-2

Table 1.

Summary of samples and the number of assigned peaks

ID	Sample	Assigned peak type	No. assigned peaks^*
I	U-¹³C,¹⁵N	Intraresidue	3545
		Sequential	606
II	[1,6-¹³C]-Glucose, U-¹⁵N	Intraresidue	1172
		Sequential	243
		Medium range (1< \|i-j\| <5)	166
		Long range (\|i-j\| ≥5)	219
		Ambiguous	205
III	[2-¹³C]-Glucose, U-¹⁵N	Intraresidue	628
		Sequential	164
		Medium range (1< \|i-j\| <5)	156
		Long range (\|i-j\| ≥5)	129
		Ambiguous	102
IV	¹³C,¹⁵N-His	Intraresidue	80
V	¹³C,¹⁵N-Tyr	Intraresidue	68
VI	Mixed-¹³C,¹⁵N-Ala/¹³C,¹⁵N-Ile-1:1	Intraresidue	508
		Medium range (1< \|i-j\| <5)	2
		Long range (\|i-j\| ≥5)	2
VII	Mixed-¹³C,¹⁵N-Ala/¹³C,¹⁵N-Val-1:1	Intraresidue	322
VIII	Diluted-N.A./U-¹³C,¹⁵N-6:1	For intermolecular contacts validation
IX	Mixed-¹³C/¹⁵N-1:1	For intermolecular contacts validation
Total Assigned Peaks			8317

Cross peaks present in different experiments are counted only once.