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. 2020 Sep 14;6(9):e04819. doi: 10.1016/j.heliyon.2020.e04819

Table 3.

Intra-day and inter-day precision and accuracy for the determination of AZI and LEVO mixtures using the proposed spectrophotometric methods.

Concentration (μg/mL)
Method Recovery % ± SDa
RSD%b
Er%c
AZI LEVO AZI LEVO AZI LEVO AZI LEVO
(a) Accuracy and intra-day precision

10 20 Direct 101.05 ± 0.59 100.95 ± 0.26 0.58 0.25 1.05 0.95
D1 100.53 ± 1.75 100.32 ± 0.69 1.75 0.69 0.53 0.32
40 10 Direct 100.75 ± 0.81 100.79 ± 0.12 0.79 0.12 0.75 0.97
D1 99.99 ± 0.91 100.32 ± 0.69 0.91 0.69 -0.01 0.32
20 20 Direct 99.69 ± 0.44 100.76 ± 0.91 0.44 0.91 -0.31 0.76
D1
100.85 ± 0.51
101.58 ± 0.91
0.51
0.90
0.85
1.58

(b) Accuracy and inter-day precision
10 20 Direct 101.44 ± 0.89 100.89 ± 0.36 0.88 0.35 1.44 0.87
D1 99.36 ± 1.01 99.92 ± 0.53 1.02 0.53 -0.64 -0.08
40 10 Direct 100.02 ± 0.22 100.83 ± 0.33 0.22 0.33 0.02 0.83
D1 100.57 ± 1.16 100.25 ± 0.64 1.15 0.64 0.57 0.25
20 20 Direct 101.53 ± 1.12 98.70 ± 0.69 1.09 0.69 1.53 -1.29
D1 101.14 ± 0.88 101.27 ± 1.13 0.87 1.12 1.14 1.27

(a) is standard deviation, (b) is percentage relative standard deviation and (c) is percentage error.