Table 1.

Yields and melting points of amides (3) when using the B(OCH₃)₃ amidation method.

Cmpd	R1	R2	Yield [%]	Mp [°C]
3 a	H	H	98	108–110
3 b	4‐F	H	89	114–116
3 c	4‐Cl	H	85	135–136
3 d	4‐Cl	Cl	84	126–128
3 e	2,4‐diCl	H	100	78–80
3 f	2,4‐diCl	Cl	40	106–108
3 g	4‐CH3	H	100	96–98
3 h	4‐CF3	H	34	104–106
3 i	4‐OCH3	H	98	126–128
3 j	3,4‐diOCH3	H	83	116–118
3 k	NHBoc	H	79	118–120