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. 2020 Aug 10;142(36):15386–15395. doi: 10.1021/jacs.0c06329

Figure 1.

Figure 1

(a) Pawley fit of the experimental PXRD pattern (λ = 1.5406 Å) of PCN-226, which shows a good agreement. (b and d) Reconstructed 3D reciprocal lattice of PCN-226(Cu) and PCN-226(Co), respectively. (c and e) The particles from which the cRED data were collected. (f and g) The hk0 reciprocal planes of PCN-226(Cu) and PCN-226(Co), respectively, showing a similar intensity distribution. (h) HRTEM image of PCN-226(Cu) along the [010] direction that shows a rectangular pore packing with d200 = 18.32 Å and d002 = 16.18 Å (calculated d200 = 18.53 Å and d002 = 16.25 Å). Inset: Fourier transform of the image. (i) Symmetry imposed HRTEM image from the region highlighted by the red square in (h). The structural model of PCN-226(Cu) is superimposed in the image to show the good agreement.