Table 10.
Summary of MOF synthesized by tubular flow reactor.
Energy source | MOF | Residence time (min) | Tube material | Tube size | Temperature (℃) | Solvent | STY (kg m−3 day−1) | Productivity (g h−1) | Yield (%) | Surface area (m2 g−1) | Ref |
---|---|---|---|---|---|---|---|---|---|---|---|
Heat | HKUST-1 (macroscale) | 1.2 | PFA | 1.0 mm ID/20 mL | 140 | EtOH | 4,533 | 61.2 | 100 | 1805 | [127] |
Heat | HKUST-1 (mesoscale) | 10 | PFA | 1.0 mm ID/20 mL | 80 | EtOH | 592 | 1.48 | 74 | 1852 | [127] |
Heat | UiO66 (mesoscale) | 10 | PFA | 1.0 mm ID/20 mL | 130 | DMF | 672 | 1.68 | 67 | 1186 | [127] |
Heat | NOTT-400 (mesoscale) | 115 | PFA | 1.0 mm ID/30 mL | 85 | DMF/THF/water | 741 | 2.78 | 61 | 1078 | [127] |
Heat | Al-Fum | 1 | Stainless-steel | 1.0 mm ID/10 mL | 65 | water | 81,120 | – | – | 1070 | [128] |
Heat | Al-Fum | 1.2 | Stainless-steel | 6.0 mm ID/107 mL | 65 | water | 73,009 | – | – | 1015 | [128] |
Heat | Al-Fum | 0.9 | Stainless-steel | 4.5 mm ID/374 mL | 65 | water | 75,247 | – | – | 1082 | [128] |
Heat | Al-Fum | 1 | Stainless-steel | 10.9 mm ID/1394mL | 65 | water | 97,159 | 5,600 | – | 1054 | [128] |
Heat | UiO-66 | 0.44 | – | 0.8 mm ID | 120 | DMF | – | – | – | 1206 | [130] |
Heat | ZIF-8 | 15 s | PFA | 1.6 mm/3mL | RT | MeOH/NH3 | 210,000 | 15,360 | 54 | 1770 | [131] |
Heat | Ce-BDC | 30 s | Stainless-steel | 0.5 mm ID/1m | 250 | DMF | – | – | – | – | [132] |
Microwave | UiO-66 | 7 (mw: 73 min) | PTFE | 4.35 mm ID/53 mL | 200 W,3bar | DMF | 7,204 | 14.4 | 94 | 1052 | [129] |
Microwave | MIL-53(Al) | 4 (mw: 34 min) | PTFE | 4.35 mm ID/53 mL | 200 W, 6 bar | DMF | 3,618 | 7.1 | 65 | 1376 | [129] |
Microwave | HKUST-1 | 1 (mw: 17 min) | PTFE | 4.35 mm ID/29.6 mL | 360 W,6bar | DMF | 64,800 | 79.4 | 96 | 1550 | [129] |