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. 2020 Aug 23;25(17):3831. doi: 10.3390/molecules25173831

Table 3.

Chemical classes or constituents found in C. ferrea extracts.

Part Used Solvent Analytical Technique Constituents Citations
Leafs Cyclohexane CG/MS Octacosane, docosane, and heptacosan [8]
Leafs Water HPLC Ellagic acid and gallic [7]
Leafs Water at 25 and 100 °C HPLC-DAD Gallic acid, caffeic and ellagic epicatechin, quercetin, and luteolin and catechin [48]
Leafs Ethanol at 70% HPLC Ellagic acid and gallic, orientin and isovitexin [49]
Leafs Ethanol at 70% NMR 1D e 2D Gallic acid, brevifolin carboxylic acid, and brevifolin [50]
Barks and seeds Ethanol at 70% HPLC Ellagic acid [51]
Barks Water at 25 and 100 °C HPLC-DAD Gallic, caffeic and ellagic acids, catechin, epicatechin and quercetin [48]
Barks Water RP-HPLC Ellagic acid and gallic [52]
Barks Ethanol and water LC-MS/MS Kaempferol, quinolinic acid and gallic [53]
Fruit Ethanol at 96% LC-HRMS/MS Corilagin and ellagic acid and gallic [1]
Fruit Water, ethanol at 20–80% HPLC-DAD Ellagic acid and gallic [7]
Fruit Ethanol HPLC Ellagic acid and gallic [54]
Fruit Water HPTLC e HPLC Ellagic acid and gallic [55]
Pods N-hexane GC-MS N-dodecanol, myristic acid, methyl palmitate, palmitic acid [56]
Pods Chloroform GC-MS n-valeric acid, caproic acid, heptanoic acid, and octanoic acid [56]
Pods Ethyl acetate GC-MS Oxalic acid, butanedioic acid, pyrotartaric acid, and pentanoic acid [56]
Pods Alcohol at 70% GC-MS Glycerol, D-fructose, myo-inositol, and glucopyranose [56]
Pods Alcohol at 40% HPLC-MS Valonium dilactone acid, gallic acid derivatives, and ellagic acid [12]
Pods Ethanol and Water LC-MS/MS Ellagic acid, chlorogenic acid, and rutin [54]
Pods Water at 25 and 100 °C HPLC-DAD Ellagic acid and gallic, catechin, epicatechin, quercetin, and luteolin [48]

GC-MS = thin-layer chromatography and Gas Chromatography-Mass Spectrometry; HPLC-DAD = High-Performance Liquid Chromatography with Diode Array Detection; RP-HPLC = Reverse Phase High-Performance Liquid Chromatography; HPLC = High Performance Liquid Chromatography; LC-HRMS/MS = Liquid Chromatography-High Resolution Tandem Mass Spectrometry; NaOH = Sodium hydroxide; LC-MS/MS = Liquid Chromatography Coupled to Tandem Mass Spectrometry; HPLC-MS = High-Performance Liquid Chromatography coupled to Mass Spectrometry; HPTLC = High-Performance Thin Layer Chromatography; NMR = Nuclear Magnetic Resonance.