Table 1.

500 MHz, 298 K, observed transverse relaxation rates for PioC HN amide protons

δ1H (ppm)	δ15 N (ppm)	residue		R2 (s−1) AP	error (s−1) AP	R2 (s−1) IP	error (s−1) AP
		VAL	1
8.26	117.2	THR	2			11.1	0.4
8.42	123.7	LYS	3			15.4	1.3
8.43	121.8	LYS	4	23.0	6.9	19.1	1.5
8.76	122.3	ALA	5	25.8	7.3	23.4	0.8
9.08	115.2	SER	6	38.8	5.2	17.8	0.6
9.64	116.3	HIS	7	37.8	4.4	21.3	0.8
8.49	116.5	LYS	8	52.9	19.1	32.8	2.2
8.13	119.5	ASP	9	35.3	5.3	16.9	0.7
8.23	118.2	ALA	10	34.6	4.3	19.6	0.8
7.69	105.0	GLY	11	46.8	3.9	20.0	1.4
8.19	116.3	TYR	12	36.6	3.8	29.9	1.5
8.67	124.5	GLN	13	54.3	3.8	46.4	4.1
8.22	115.2	GLU	14			19.4	1.1
7.29	112.8	SER	15	21.9	5.8	21.6	1.0
		PRO	16
7.92	116.4	ASN	17	31.2	4.4	22.8	1.1
8.17	111.6	GLY	18	43.5	5.2	25.1	1.5
8.78	126.9	ALA	19	52.6	12.0	44.4	2.8
7.62	118.4	LYS	20	41.8	10.9	17.8	0.8
7.47	115.9	ARG	21	38.0	2.8	44.4	3.1
9.47	131.4	CYS	22	313.6	19.6	n.o
8.62	97.5	GLY	23	60.3	6.2	48.8	6.3
8.62	109.8	THR	24	45.9	4.1	42.0	2.8
8.36	130.0	CYS	25	65.0	5.1	44.1	7.5
9.28	131.4	ARG	26	47.9	4.9	55.5	5.3
9.62	141.7	GLN	27	221.0	15.1	n.o
7.72	123.4	PHE	28	172.3	8.4	n.o
8.19	128.2	ARG	29	39.2	5.2	44.9	3.0
		PRO	30
		PRO	31
8.15	111.8	SER	32	43.5	5.2	25.1	1.5
7.55	114.9	SER	33	43.4	4.3	24.2	0.8
8.55	129.0	CYS	34	37.5	3.9	42.5	3.7
8.36	126.0	ILE	35	84.5	5.9	65.6	26
8.75	127.6	THR	36	115.0	12.3	n.o
7.00	149.9	VAL	37	161.5	10.7	n.o
8.61	122.8	GLU	38	43.0	4.0	24.2	0.8
8.43	115.7	SER	39	35.2	8.3	19.7	1.0
		PRO	40
7.28	118.2	ILE	41	25.4	7.5	27.7	1.3
7.84	116.4	SER	42	36.7	3.8	42.8	2.4
9.12	121.2	GLU	43	24.1	3.4	19.2	0.5
7.98	116.8	ASN	44	25.7	5.2	27.4	1.5
7.20	102.6	GLY	45	55.5	3.8	46.2	6.5
7.86	113.7	TRP	46	73.1	5.0	54.8	14.8
6.47	118.9	CYS	47	182.7	11.0	n.o
6.79	115.2	ARG	48	57.9	5.3	74.0	28.6
7.74	154.7	LEU	49	168.4	12.4	n.o
6.02	119.5	TYR	50	56.6	14.3	n.o
5.46	119.0	ALA	51	216.6	42.0	n.o
8.33	109.7	GLY	52	39.4	4.4	23.0	1.3
8.43	120.2	LYS	53	24.9	5.0	18.0	0.9
8.04	128.5	ALA	54			7.7	0.3
8.53	124,0	TRP sc	46	53.1	4.2	33.9	2.1

Columns 5–6 refer to values observed with the R₂-weighted HSQC-AP experiment, columns 7–8 to values observed with an in-phase HSQC experiment with a single exponential T₂ decay prior to INEPT