| Stoe IPDS 2 diffractometer | 2962 independent reflections |
| Radiation source: sealed X-ray tube, 12 x 0.4 mm long-fine focus | 1950 reflections with I > 2σ(I) |
| Detector resolution: 6.67 pixels mm-1 | Rint = 0.048 |
| rotation method scans | θmax = 26.0°, θmin = 2.4° |
| Absorption correction: integration (X-RED32; Stoe & Cie, 2002) | h = −21→21 |
| Tmin = 0.896, Tmax = 0.983 | k = −7→7 |
| 10315 measured reflections | l = −21→19 |
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