Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C17H16N2OS |
| M r | 296.38 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 296 |
| a, b, c (Å) | 17.251 (1), 5.6849 (3), 17.3101 (11) |
| β (°) | 116.958 (4) |
| V (Å3) | 1513.14 (16) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.21 |
| Crystal size (mm) | 0.67 × 0.34 × 0.04 |
| Data collection | |
| Diffractometer | Stoe IPDS 2 |
| Absorption correction | Integration (X-RED32; Stoe & Cie, 2002 ▸) |
| T min, T max | 0.896, 0.983 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 10315, 2962, 1950 |
| R int | 0.048 |
| (sin θ/λ)max (Å−1) | 0.617 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.045, 0.099, 0.98 |
| No. of reflections | 2962 |
| No. of parameters | 191 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.14, −0.13 |