13BMD @ APS diffractometer | 253 reflections with I > 2σ(I) |
Radiation source: synchrotron | Rint = 0.055 |
/w scan | θmax = 14.8°, θmin = 3.2° |
Absorption correction: multi-scan (CrysAlisPro; Rigaku OD, 2018) | h = −11→12 |
Tmin = 0.546, Tmax = 1.000 | k = −9→8 |
592 measured reflections | l = −4→4 |
321 independent reflections |