| Crystal data |
| Chemical formula |
[Fe(C13H11N4)2] |
|
M
r
|
502.36 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
90 |
|
a, b, c (Å) |
5.7905 (3), 9.7461 (5), 10.1720 (4) |
| α, β, γ (°) |
82.064 (3), 84.754 (4), 77.739 (4) |
|
V (Å3) |
554.44 (5) |
|
Z
|
1 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.71 |
| Crystal size (mm) |
0.12 × 0.09 × 0.08 |
| |
| Data collection |
| Diffractometer |
Bruker Kappa APEXII DUO CCD |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
T
min, T
max
|
0.857, 0.945 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
7058, 4199, 3569 |
|
R
int
|
0.020 |
| (sin θ/λ)max (Å−1) |
0.769 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.041, 0.099, 1.06 |
| No. of reflections |
4199 |
| No. of parameters |
160 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.98, −0.29 |
