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. 2020 Aug 17;26(51):11722–11726. doi: 10.1002/chem.202002957

Table 1.

Experimental (δ exp) and calculated (δ cal) 31P NMR chemical shifts of compounds 5, B, 6 and 7.

5

B

6

7

δ exp/ppm

−273[a]

945[b]

1124[a]

−166[a]

δ cal/ppm

−242

1046

1221

−111

[a] Recorded in thf with C6D6 capillary at room temperature. [b] Recorded in CD2Cl2 at −20 °C.18