Table 1.

Experimental details of 2D and 3D spectra collected for backbone and sidechain assignments.

Experiment	No. of scans	Spectral window (ppm)	Complex points	Offset (ppm)
15N -HSQC&	8	16.67 × 26.318	1024 × 128	4.773 × 117.88
CBCA(CO)NH*	32	16.67 × 57.009 × 26.318	1024 × 52 × 42	4.773 × 43.75 × 117.88
HNCACB*	16	15.44 × 63.141 × 32.256	1024 × 66 × 42	4.771 × 43.718 × 117.666
HNCO*	32	16.285 × 13.924 × 29.619	1024 × 48 × 48	4.773 × 175.945 × 117.692
HN(CO)CA*	52	16.67 × 27.841 × 26.318	800 × 64 × 42	4.773 × 55.8 × 117.88
HNCA*	52	16.67 × 27.841 × 26.318	800 × 64 × 42	4.773 × 55.8 × 117.88
1H-13C-HSQC-CT$	16	20.04 × 72.918	1024 × 256	4.797 × 42.964
C(CO)NH*	64	20.04 × 76.233 × 26.318	1024 × 64 × 32	4.797 × 42.964 × 117.904
HBHA(CO)NH#	32	20.04 × 6.0 × 26.318	1024 × 60 × 40	4.797 × 4.797 × 117.904
H(CCO)NH#	64	20.04 × 8.335 × 26.318	1024 × 64 × 32	4.797 × 4.797 × 117.904
HC(C)H-TOCSY@	8	20.04 × 8.335 × 72.925	1024 × 64 × 64	4.797 × 4.797 × 42.964
Aromatic 1H, 13CHSQC-CT$	32	16.669 × 29.167	1024 × 70	4.797 × 125.569
Aromatic Cβ-13CHSQC-CT$	32	16.669 × 18.561	1024 × 124	4.797 × 35.186
(HB)CB(CGCD)HD$	512	16.669 × 19.887	1024 × 23	4.797 × 35.186
(HB)CB(CGCDCE)HE$	512	16.669 × 19.887	1024 × 23	4.797 × 35.186
Aromatic HCCHTOCSY@	16	20.04 × 3.334 × 29.165	1024 × 64 × 48	4.773 × 4.773 × 125.552

^&(¹H × ¹⁵N);

^*(¹H × ¹³C × ¹⁵N);

^$(¹H × ¹³C);

^#(¹H × ¹H × ¹⁵N);

^@(¹H × ¹H × ¹³C)