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. 2020 Sep 22;9(9):903. doi: 10.3390/antiox9090903

Table 2.

UPLC analysis of phenolic compounds in spice extracts (mg/kg DW).

Phenolic Compounds Nutmeg Allspice Bay Leaf Black Seed Cloves Caraway Cardamom
protocatechuic acid 0.23 a 0.36 a <LOD 1.26 a 79.57 c 0.22 a 12.57 b
2,5-dihydroxybenzoic acid <LOD <LOD 16.52 d 1.23 bc 1.33 c <LOD 0.23 ab
4-hyrdoxybenzoic acid 0.19 a <LOD 36.50 c <LOD 40.12 d 10.69 b 2.36 a
gallic acid 10.24 c <LOD <LOD <LOD 0.36 a 0.16 a 1.39 b
syryngic acid 10.84 c 0.75 ab 0.66 ab 12.66 d 1.22 b <LOD <LOD
t-cinnamic acid 3.95 b 0.00 19.62 e <LOD 29.50 d 6.58 c 1.49 a
caffeic acid 2.30 a <LOD <LOD <LOD 52.90 b 59.30 c <LOD
p-coumaric acid <LOD <LOD <LOD 29.54 b 5.30 a <LOD <LOD
ferulic acid <LOD <LOD 0.23 a <LOD 2.10 b <LOD <LOD
sinapic acid 0.22 ab 0.06 a 1.95 d 3.45 e <LOD 0.59 b 1.46 c
chlorogenic acid 0.06 a 0.49 a 0.56 a 0.37 a 10.20 b 0.11 a 0.46 a
total phenolic acids 27.97 b 1.16 a 75.47 d 48.14 c 212.4 e 77.52 d 19.50 b
eriodictyol 0.26 a <LOD 0.45 b <LOD <LOD 1.13 c 0.22 a
apigenin 12.83 c 0.36 a 12.65 c <LOD 0.07 a 0.06 a 6.33 b
luteolin 0.23 a 0.36 a 10.54 b 19.50 c 0.06 a 12.36 b 27.50 d
catechin 57.20 b 0.23 a 1.26 a <LOD 0.39 a <LOD 1.68 a
rutin <LOD 7.25 c 1.95 b 0.13 a <LOD <LOD <LOD
kaempferol 0.44 a 10.65 c 0.11 a 4.52 b 0.05 a 0.26 a <LOD

All values are mean of the three replicates. (a–e) means with the same superscript within the same row are not different (p > 0.05, Duncans’s test). LOD—limit of detection.