Table 8.
Data analysis of validation tests.
| Release Tests | Permeation Tests | ||
|---|---|---|---|
| Concentration range | 0.596–19.2 μg/mL | 0.632–24.96 μg/ml | |
| Calibration curve | y = 785579.7x − 257656 | y = 604067.2x − 206475.1 | |
| R2 | 0.9999 | 0.9999 | |
| NA | Limit of detection (LOD) | 0.196 | 0.086 |
| Limit of quantitation (LOQ) | 0.595 | 0.261 | |
| Mean %Recovery | >95.6% | >96.1 | |
| Mean %RSD | 3.1 | 2.01 | |
| Concentration range | 1.184–20.16 μg/ml | 1.232–184.8 μg/ml | |
| Calibration curve | 282969.4x − 6572 | 260781.98x − 49662 | |
| THCl | R2 | 0.9992 | 0.9996 |
| LOD | 0.336 | 0.591 | |
| LOQ | 1.017 | 1.789 | |
| Mean %Recovery | >97.3 | >98.4 | |
| Mean %RSD average | 3.7 | 2.51 |