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. 2020 Aug 1;29(11):1573–1586. doi: 10.1007/s10068-020-00798-4

Table 3.

Recovery and relative standard deviation (RSD) at three concentrations of pesticides in livestock products

Pesticide Fortified Concentration (mg/kg) Beef Pork Chicken Eggs Milk
Recovery (%) RSD (%) Recovery (%) RSD (%) Recovery (%) RSD (%) Recovery (%) RSD (%) Recovery (%) RSD (%)
Aldrin 0.005 71.6 10.1 70.8 8.79 76.7 13.2 87.6 10.0 85.7 11.4
0.01 72.3 3.73 70.9 6.57 85.5 6.65 85.6 16.3 95.5 8.05
0.1 70.4 6.42 70.1 4.45 90.2 12.3 90.0 11.7 93.7 2.93
BHC-gamma 0.005 72.7 16.7 70.6 6.99 75.4 15.9 95.1 1.26 92.2 8.69
0.01 72.0 3.90 70.5 6.30 77.8 9.09 85.0 11.0 88.7 4.31
0.1 72.5 9.80 74.4 6.64 73.2 18.6 90.0 8.45 88.9 3.98
Bifenthrin 0.005 75.1 8.26 82.3 4.83 89.4 4.96 116 4.68 90.6 5.76
0.01 79.9 5.88 76.2 6.57 90.0 3.90 111 13.1 86.1 3.81
0.1 75.8 6.87 85.9 3.60 116 3.08 120 10.7 84.2 2.99
Chinomethionat 0.005 71.2 8.44 72.0 10.0 103 7.86 73.0 3.61 95.1 9.34
0.01 75.8 4.85 70.1 9.41 105 6.90 71.1 6.43 95.3 3.67
0.1 74.5 7.12 74.3 12.4 114 9.62 70.6 14.7 90.9 3.67
Chlordane-cis 0.005 102 9.12 77.8 15.1 81.1 17.2 110 12.7 100 11.7
0.01 92.4 5.30 73.9 12.9 86.9 12.6 97.7 15.9 97.4 3.35
0.1 71.4 6.16 74.3 17.1 105 7.18 77.1 19.5 94.7 5.90
Chlordane-trans 0.005 74.6 10.8 78.2 14.1 85.9 14.2 74.9 2.43 73.3 12.3
0.01 72.5 5.31 77.3 12.1 89.2 9.88 71.5 11.4 76.9 12.2
0.1 70.5 10.0 83.2 7.13 116 8.81 71.0 11.9 91.1 8.42
Chlorfenvinphos 0.005 76.6 12.7 83.4 6.44 85.3 9.43 78.4 13.7 92.9 7.21
0.01 81.0 5.37 74.2 6.73 85.9 4.65 84.3 8.16 84.2 3.65
0.1 70.6 8.56 86.8 3.78 85.4 8.56 87.5 13.3 95.9 3.10
Chlorpyrifos 0.005 73.4 10.8 86.5 9.52 86.7 7.38 116 6.27 95.2 9.80
0.01 78.9 1.56 72.2 7.30 91.8 8.62 104 12.0 95.4 4.60
0.1 74.7 19.1 81.5 2.76 103 5.07 111 10.9 97.2 3.34
Chlorpyrifos-methyl 0.005 81.4 12.8 95.3 6.84 81.9 13.2 91.7 15.2 81.9 10.6
0.01 92.6 5.47 80.0 4.25 84.0 4.21 92.8 16.4 87.9 8.33
0.1 75.0 9.02 97.8 2.79 86.7 14.7 99.1 8.36 95.8 1.81
Cypermethrin 0.005 88.6 3.04 104 8.01 86.9 5.25 109 10.4 89.7 4.64
0.01 93.8 4.66 93.5 7.78 90.6 3.58 119 16.2 84.6 2.38
0.1 77.9 7.29 101 3.91 109 4.99 120 9.76 92.2 5.20
p,p′-DDD 0.005 72.7 14.3 81.2 3.91 87.3 9.25 114 2.93 93.5 5.96
0.01 71.4 5.03 74.7 7.19 89.2 8.52 114 13.4 89.1 3.77
0.1 70.3 11.6 89.1 4.52 112 5.24 118 12.1 95.2 4.31
p,p′-DDE 0.005 70.5 8.81 71.8 8.35 88.9 6.90 108 0.44 89.6 4.63
0.01 70.3 4.25 70.9 7.94 93.0 5.77 91.7 16.1 85.5 2.70
0.1 70.2 6.96 71.1 13.9 118 3.81 94.9 13.0 72.6 3.73
o, p-DDT 0.005 113 11.3 74.1 3.75 85.5 5.17 82.4 9.18 80.4 7.57
0.01 71.3 18.1 75.7 6.71 83.8 9.56 75.8 15.8 90.1 2.73
0.1 70.2 16.3 77.1 7.66 103 1.55 74.9 8.90 79.2 3.72
p,p′-DDT 0.005 70.7 14.7 75.7 5.15 73.8 6.02 102 19.2 74.9 5.57
0.01 75.9 8.64 78.6 6.60 71.3 3.25 106 4.92 70.1 5.01
0.1 72.2 13.1 75.9 5.39 89.4 8.10 88.6 12.2 72.6 3.73
Diazinon 0.005 72.0 12.7 71.3 7.86 72.0 12.7 99.4 3.99 71.3 15.4
0.01 76.6 2.41 70.6 8.41 76.6 2.41 88.2 10.8 73.4 5.54
0.1 74.6 7.84 77.9 5.71 74.6 7.84 94.4 12.4 70.5 6.99
Dichlorvos 0.005 103 13.1 76.5 19.8 73.9 3.04 77.5 11.9 73.5 13.1
0.01 110 4.92 74.4 11.8 72.1 8.02 70.9 9.74 71.9 5.19
0.1 113 5.22 77.7 14.5 70.2 3.38 71.5 19.6 70.6 7.90
Dieldrin 0.005 77.9 15.2 116 7.41 83.9 11.0 98.2 2.59 86.6 7.09
0.01 72.4 8.69 70.9 10.8 87.6 10.6 81.7 8.80 88.1 3.72
0.1 76.2 7.99 74.8 7.28 102 3.75 85.1 10.6 81.4 3.17
Dimethoate 0.005 79.5 15.0 87.4 8.86 90.3 7.16 91.5 15.2 76.8 8.85
0.01 90.4 5.61 86.8 6.90 82.9 11.2 104 13.7 70.9 6.08
0.1 81.7 11.3 104 1.86 116 5.65 96.8 8.09 82.4 3.54
Diphenylamine 0.005 113 11.5 70.5 17.7 107 13.1 84.3 3.41 80.9 11.8
0.01 111 3.33 112 9.94 114 11.4 75.7 4.71 94.5 10.9
0.1 88.7 6.54 97.8 11.0 107 5.25 72.4 6.48 93.8 9.91
Disulfoton 0.005 96.7 13.1 91.9 4.07 71.4 11.4 99.5 2.16 81.0 7.38
0.01 102 8.19 105 13.5 79.9 5.16 89.9 11.7 78.9 4.22
0.1 86.8 8.09 79.7 13.2 73.3 8.91 77.1 9.07 77.2 5.68
Edifenphos 0.005 73.0 15.3 84.3 8.68 75.1 4.58 77.1 9.02 75.5 6.40
0.01 82.0 4.13 75.9 13.1 75.8 6.13 70.5 10.6 71.9 3.86
0.1 74.9 12.4 99.6 10.3 97.9 5.57 79.6 15.3 71.3 5.40
Endosulfan alpha 0.005 70.9 15.8 77.2 18.5 91.6 9.83 102 3.44 97.8 10.5
0.01 72.8 12.0 72.5 12.7 97.7 13.4 98.0 12.3 96.3 3.49
0.1 71.7 14.6 75.5 14.9 107 9.28 71.0 8.24 94.3 2.34
Endosulfan beta 0.005 108 10.7 77.4 16.2 83.6 12.4 114 2.22 95.9 12.7
0.01 71.2 19.7 70.6 5.92 90.4 12.4 95.2 15.8 83.4 6.16
0.1 71.6 10.7 79.4 2.83 109 2.94 114 8.18 95.5 4.54
Endosulfan sulfate 0.005 74.4 12.3 84.1 6.82 71.7 4.12 73.8 8.69 99.9 10.9
0.01 70.5 6.40 77.6 10.1 80.5 4.23 86.5 18.1 91.7 4.17
0.1 70.6 12.2 87.8 8.92 114 6.35 84.9 9.86 92.1 2.88
Endrin 0.005 70.7 15.7 75.9 11.3 84.3 15.1 93.8 15.7 92.2 7.15
0.01 77.0 8.13 70.8 5.34 86.7 6.96 86.5 18.1 79.9 5.68
0.1 71.7 12.9 77.0 5.69 99.2 4.27 84.9 9.86 79.5 2.71
Ethion 0.005 89.8 11.7 74.3 19.9 76.2 10.6 115 0.23 92.9 11.5
0.01 78.1 11.9 71.5 17.8 77.8 12.0 110 0.52 84.1 5.41
0.1 90.0 3.44 91.2 19.1 99.3 4.18 115 6.29 96.2 2.07
Etrimfos 0.005 70.1 11.9 76.8 5.42 70.6 17.7 97.5 0.24 76.7 8.09
0.01 73.2 3.05 77.4 5.79 70.5 2.28 83.5 9.61 76.7 6.27
0.1 72.5 9.04 74.8 4.10 70.2 7.20 88.0 6.32 76.3 4.67
Fenarimol 0.005 75.6 10.8 85.4 7.38 80.6 14.2 111 11.9 93.4 4.09
0.01 84.3 6.30 81.3 6.91 88.0 2.07 111 12.0 94.9 2.10
0.1 71.6 7.77 89.4 5.12 102 8.56 119 10.0 96.3 3.28
Fenbuconazole 0.005 84.2 9.81 88.5 7.16 82.2 14.7 119 15.4 85.3 9.05
0.01 90.2 6.05 86.2 6.99 82.0 2.72 119 9.62 80.2 2.77
0.1 76.8 6.88 95.0 4.22 108 9.73 117 12.3 87.2 1.55
Fenitrothion 0.005 72.6 13.4 70.8 4.83 80.0 8.37 111 2.40 83.2 9.77
0.01 80.5 4.89 80.1 5.49 87.3 9.80 95.1 8.32 86.0 4.91
0.1 71.0 11.4 90.7 6.26 100 8.56 72.4 18.0 85.4 5.59
Fenpropathrin 0.005 79.0 7.11 82.3 4.42 89.0 5.91 110 8.43 90.2 3.95
0.01 83.8 4.76 79.4 7.48 88.9 7.12 113 11.2 88.4 3.41
0.1 73.6 7.61 90.3 3.24 115 0.57 119 9.94 92.7 4.01
Fensulfothion 0.005 73.7 8.67 72.3 18.7 75.7 9.16 73.8 12.2 72.4 16.6
0.01 71.3 11.7 71.3 7.77 82.8 10.7 78.5 5.63 75.9 11.5
0.1 70.8 10.5 72.4 10.9 103 11.8 70.4 10.3 71.1 14.7
Fenthion 0.005 72.8 10.3 72.0 7.33 76.6 6.90 108 2.52 93.0 9.64
0.01 72.6 4.02 71.1 4.74 76.6 9.12 87.4 12.1 83.6 4.05
0.1 72.2 8.18 71.9 8.97 79.1 12.7 93.9 9.45 90.3 4.73
Fenvalerate 0.005 87.2 8.51 99.4 2.76 88.1 6.90 111 15.6 98.4 5.29
0.01 89.9 5.29 91.9 7.08 87.6 5.19 107 14.5 91.8 2.92
0.1 76.3 7.14 100 3.69 109 6.90 113 9.61 82.0 3.78
Flusilazole 0.005 76.3 11.0 74.6 8.31 87.1 10.6 114 6.34 91.0 6.69
0.01 82.5 3.87 78.2 6.36 86.7 6.50 107 13.8 82.0 4.72
0.1 70.2 9.68 80.3 4.51 116 6.50 113 11.9 89.0 1.92
Heptachlor 0.005 71.9 15.0 74.5 6.95 73.3 1.73 92.6 2.55 89.4 9.89
0.01 72.1 3.70 75.5 7.26 77.9 8.80 80.7 10.4 83.6 9.75
0.1 70.5 7.83 72.1 10.3 97.6 3.22 78.7 7.59 93.2 6.93
Heptachlor epoxide 0.005 73.5 16.3 75.5 15.4 80.0 12.0 85.3 1.95 95.0 12.3
0.01 70.6 10.4 71.0 9.65 95.8 11.3 87.9 5.46 95.6 3.71
0.1 72.0 6.90 79.3 3.61 102 8.02 101 7.50 94.6 1.22
Isofenphos 0.005 76.0 6.87 80.2 6.66 85.0 9.72 96.0 3.46 93.6 7.31
0.01 77.1 4.21 72.6 7.13 83.9 6.18 87.6 11.0 89.8 4.43
0.1 75.3 9.32 81.3 2.13 86.4 10.5 99.1 10.2 90.7 2.54
keto Endrin 0.005 97.6 17.0 70.2 9.77 78.7 11.5 107 5.14 89.7 7.45
0.01 70.6 15.2 70.2 6.71 80.2 8.10 91.3 14.3 97.9 4.85
0.1 71.3 10.9 71.8 14.4 109 2.07 97.2 11.3 95.4 3.43
Kresoxim methyl 0.005 71.1 9.98 81.1 6.46 82.4 15.2 118 4.51 90.9 6.34
0.01 70.7 4.17 72.4 7.14 86.5 11.2 112 15.3 72.4 6.73
0.1 70.8 7.64 72.7 11.4 106 9.76 113 15.7 87.8 5.70
Mecarbam 0.005 81.0 9.76 94.1 15.7 89.8 6.61 112 3.00 98.7 11.7
0.01 76.0 2.82 82.5 19.9 85.3 14.8 110 2.88 93.0 6.21
0.1 71.7 9.78 81.5 3.76 113 6.41 106 9.67 89.4 3.20
Methacrifos 0.005 110 12.0 70.4 17.9 81.0 9.76 81.9 2.93 70.2 12.0
0.01 72.5 19.4 71.3 4.74 76.0 2.82 85.8 12.2 70.4 9.82
0.1 72.5 19.1 76.5 8.05 71.7 9.78 84.7 5.89 73.2 11.1
Methidathion 0.005 71.8 10.0 71.1 10.8 105 8.20 70.1 12.4 94.4 6.69
0.01 71.4 4.93 70.4 7.06 101 4.92 71.1 10.7 91.5 3.27
0.1 75.7 7.83 71.8 7.90 120 9.98 71.5 13.7 88.0 2.56
Myclobutanil 0.005 75.3 9.05 77.1 9.11 83.0 18.2 117 15.8 86.8 7.09
0.01 71.1 5.68 70.5 7.01 85.8 8.41 118 16.2 86.9 5.77
0.1 71.2 7.40 77.6 8.19 112 8.03 115 13.4 92.3 4.62
Oxychlordane 0.005 72.3 11.6 73.8 8.78 93.5 9.65 102 6.83 92.5 11.6
0.01 72.0 8.33 72.0 10.8 90.0 4.28 93.5 6.20 93.9 4.21
0.1 72.3 9.81 75.5 5.06 102 10.4 105 10.5 91.2 3.77
Penconazole 0.005 79.8 8.54 92.4 10.6 97.5 6.41 109 3.16 93.8 8.93
0.01 81.4 7.29 82.5 8.07 91.7 8.28 101 10.5 95.4 3.09
0.1 72.7 7.94 93.2 3.12 118 4.12 110 10.3 88.5 3.03
Pentachloraniline 0.005 71.3 9.68 75.9 4.57 82.6 13.7 84.0 0.33 89.1 11.5
0.01 70.2 2.78 71.6 8.05 86.5 2.78 81.3 10.6 76.7 4.73
0.1 71.6 5.47 80.1 3.16 87.8 11.7 83.9 9.23 84.7 11.7
Pentachlorothioanisole 0.005 70.1 19.2 72.1 3.15 85.2 2.55 90.8 9.53 82.4 5.68
0.01 70.6 11.7 71.4 4.40 87.0 5.37 83.6 14.0 92.0 5.98
0.1 71.9 12.9 78.1 4.55 97.5 17.5 86.5 9.59 99.0 6.30
Permethrin 0.005 77.2 4.96 72.8 4.09 94.4 4.56 117 7.87 81.9 9.70
0.01 73.2 6.01 72.2 8.39 93.7 9.63 111 11.2 76.1 2.05
0.1 75.4 6.93 94.2 4.17 110 6.54 116 10.1 80.4 3.53
Phenthoate 0.005 73.2 10.6 80.3 7.18 90.4 8.99 100 2.26 94.0 6.86
0.01 78.6 4.52 70.1 7.04 90.2 7.38 93.7 11.7 86.8 5.46
0.1 75.4 7.54 79.4 1.94 88.4 7.84 94.6 10.8 91.5 4.74
Phorate 0.005 86.8 17.3 70.3 10.8 88.4 15.8 93.8 2.75 86.6 8.16
0.01 110 5.27 84.9 3.96 118 7.47 87.3 11.8 80.9 6.75
0.1 92.3 5.20 74.3 4.28 116 5.69 90.4 6.63 80.6 4.99
Phosalone 0.005 79.6 13.4 91.3 3.28 83.7 11.8 105 11.0 83.1 4.47
0.01 84.6 4.40 83.2 7.35 88.5 6.03 93.4 12.0 90.7 6.96
0.1 71.0 9.27 92.4 3.11 107 3.90 101 10.7 96.4 5.71
Phosmet 0.005 75.3 13.2 87.6 6.97 73.4 9.46 93.2 19.8 90.1 2.91
0.01 82.8 7.43 84.1 8.68 74.4 5.84 83.7 10.6 85.2 3.14
0.1 72.6 10.8 99.4 3.45 99.9 5.64 87.2 14.2 87.0 3.19
Primicarb 0.005 72.4 10.5 76.9 9.61 76.1 15.4 101 9.37 73.3 12.6
0.01 76.2 3.87 71.1 6.77 72.0 1.69 92.0 8.83 71.3 7.73
0.1 81.5 6.87 79.6 3.54 86.1 11.7 95.6 7.88 74.3 6.11
Primiphos methyl 0.005 70.1 18.3 74.4 11.3 72.5 12.0 72.4 8.62 74.9 15.5
0.01 77.4 4.18 74.8 9.06 78.9 6.27 74.1 6.52 71.3 6.11
0.1 72.4 11.6 83.6 5.50 85.8 10.2 72.7 16.6 72.5 3.74
Prochloraz 0.005 77.1 10.0 81.7 7.64 80.1 12.8 115 9.44 79.5 9.51
0.01 82.9 6.66 79.0 8.18 77.8 5.30 96.3 11.8 74.0 6.81
0.1 70.2 8.38 88.0 5.25 97.0 8.77 98.3 13.6 77.3 2.69
Profenphos 0.005 118 9.12 92.4 15.9 118 9.12 80.2 10.6 71.1 19.7
0.01 94.9 6.01 76.0 16.9 94.9 6.01 91.2 11.2 71.0 13.7
0.1 70.3 14.8 72.7 17.0 70.3 14.5 85.3 12.3 90.0 4.71
Propagite 0.005 104 16.3 74.2 19.4 70.2 1.78 70.1 3.05 74.3 8.53
0.01 75.2 15.2 70.6 14.5 70.5 3.67 74.2 4.77 75.1 6.94
0.1 72.6 6.96 73.3 4.24 70.0 4.60 71.2 2.98 77.2 3.16
Propiconazole 0.005 71.6 16.1 85.9 19.9 71.6 16.1 107 14.8 92.8 10.9
0.01 109 6.59 77.8 15.4 109 6.59 84.2 15.2 70.9 5.02
0.1 71.7 7.38 71.0 3.22 71.7 7.38 73.0 14.5 73.9 3.13
Pyriproxyfen 0.005 84.9 10.2 86.7 5.13 74.1 15.1 112 17.1 87.9 8.26
0.01 85.2 7.02 80.1 6.85 83.7 6.06 113 14.5 91.6 5.18
0.1 71.8 7.75 88.0 3.61 114 4.91 119 9.96 89.9 6.26
Quintozene 0.005 102 14.2 74.0 6.62 77.2 15.2 81.4 2.16 88.0 7.68
0.01 99.2 4.33 75.5 7.47 79.6 5.55 77.0 13.6 87.4 5.60
0.1 82.3 4.98 90.6 1.71 102 1.30 77.0 6.53 86.8 3.41
Terbufos 0.005 79.3 15.0 112 10.1 79.3 15.0 81.4 18.4 82.2 11.4
0.01 77.3 18.2 83.0 5.20 77.3 18.2 104 7.62 105 11.2
0.1 76.1 11.2 87.0 3.49 76.1 11.2 89.2 8.83 85.1 5.02
Triadimefon 0.005 78.1 13.0 79.9 10.2 86.6 12.6 109 6.78 82.9 13.0
0.01 79.6 9.36 72.0 7.33 86.2 2.41 99.4 8.45 76.5 6.35
0.1 71.2 7.80 84.1 4.13 109 7.23 106 10.7 87.3 3.08
Triadimenol 0.005 83.3 15.1 99.7 11.9 86.7 5.41 105 6.69 72.2 4.37
0.01 73.9 1.79 71.7 10.9 72.6 12.5 115 4.99 73.1 4.31
0.1 76.2 6.03 73.5 8.46 104 12.3 117 9.98 75.1 3.10
Trizaofos 0.005 81.0 7.93 83.3 7.49 74.1 9.60 118 9.84 89.7 7.13
0.01 84.6 5.43 78.9 6.17 81.7 12.7 115 11.1 83.9 4.77
0.1 71.4 6.89 88.1 3.71 101 7.41 118 10.9 93.7 4.27
Vinclozolin 0.005 90.6 8.08 82.2 2.74 83.8 14.3 100 1.92 95.1 7.07
0.01 92.8 4.24 82.9 8.53 86.0 5.35 97.9 10.1 89.1 4.20
0.1 79.9 8.10 95.2 1.94 96.3 6.47 99.2 9.03 85.3 3.04