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. 2020 Sep 11;25(18):4170. doi: 10.3390/molecules25184170

Table 1.

The experimental conditions of CO2 supercritical fluid extraction (CO2-SFE) and yield of Rana chensinensis ovum oil (RCOO) based on the Box–Behnken Design (BBD).

No. X1: Pressure (MPa) X2: Flow (L/h) X3: Temperature (°C) X4: Time (min) Actual Yield (%) Predicted Yield (%) Residual (%)
SFE1 35 75 47 30 8.69 8.05 0.64
SFE2 25 75 47 90 11.48 11.31 0.17
SFE3 35 100 47 90 11.92 12.19 −0.27
SFE4 25 100 32 90 11.99 11.36 0.63
SFE5 15 100 47 90 9.08 10.09 −1.01
SFE6 25 100 62 90 11.69 10.61 1.08
SFE7 25 50 47 150 11.51 11.12 0.39
SFE8 35 75 32 90 10.16 9.65 0.51
SFE9 25 75 32 30 3.81 5.20 −1.39
SFE10 35 75 47 150 13.06 13.42 −0.36
SFE11 15 75 47 30 3.03 1.92 1.11
SFE12 25 50 62 90 7.55 7.42 0.13
SFE13 25 75 47 90 11.55 11.31 0.24
SFE14 25 75 62 150 12.56 12.20 0.36
SFE15 25 50 47 30 2.36 1.77 0.59
SFE16 25 100 47 30 7.96 8.07 −0.11
SFE17 15 75 47 150 10.65 10.53 0.12
SFE18 25 75 47 90 10.89 11.31 −0.42
SFE19 15 75 32 90 9.24 8.48 0.76
SFE20 25 75 32 150 11.25 11.44 −0.19
SFE21 25 100 47 150 12.39 12.71 −0.32
SFE22 25 75 62 30 3.61 4.46 −0.85
SFE23 35 50 47 90 10.62 10.65 −0.03
SFE24 15 50 47 90 2.98 3.74 −0.76
SFE25 35 75 62 90 12.51 13.00 −0.49
SFE26 15 75 62 90 4.93 5.16 −0.23
SFE27 25 50 32 90 6.32 6.65 −0.33

X1, X2, X3, and X4 are the codes for pressure, flow, temperature, and time in the BBD model, respectively.