Table 2.
Accuracy and Precision (n = 5, Three days) | LLOQ (25 nM) | MQC (500 nM) | HQC (800 nM) | |
---|---|---|---|---|
1st day Intraday | Bias (mean, n = 5) | 15.41 | −6.30 | −1.09 |
Average Percent Recovery | 115.41% | 93.70% | 98.91% | |
S.D. | 14.55 | 2.01 | 3.57 | |
% R.S.D | 12.61 | 2.14 | 3.64 | |
2nd day Intraday | Bias (mean, n = 5) | 10.34 | 1.49 | −0.10 |
Average Percent Recovery | 110.34% | 101.49% | 99.90% | |
S.D. | 15.37 | 1.90 | 1.82 | |
% R.S.D | 13.92 | 1.87 | 1.82 | |
3rd day Intraday | Bias (mean, n = 5) | 13.80 | 0.98 | −0.91 |
Average Percent Recovery | 113.80% | 100.98% | 99.09% | |
S.D. | 9.57 | 1.83 | 2.62 | |
% R.S.D | 8.41 | 1.81 | 2.64 | |
Interday | Bias (mean, n = 15) | 13.40 | −1.30 | −1.01 |
Average Percent Recovery | 113.40% | 98.70% | 98.99% | |
S.D. | 13.41 | 4.02 | 2.89 | |
% R.S.D | 11.83 | 4.07 | 2.92 |