Table 4a:
Uncertainty budgets for the SIRTI measurement of the 18F ampoules
Uncertainty contributions due to | Comments | Evaluation method | Relative standard uncert. × 104 |
---|---|---|---|
18F to 94Nb meas. ratio including live-time, background, decay corrections and threshold setting | Standard uncertainty of the weighted mean of 33 measurements, taking into account the correlation due to the 18F half-life | A | 2.4 |
Long-term stability of the SIRTI | Weighted standard deviation of 85 series, each series consisting of 10 measurements | A | 0.3 |
Nb-l bias from the mean since 2007 | Relative difference from the mean | B | 1.8 |
Effect of decay on the live-time correction | Maximum measurement duration evaluated from [12] | B | < l |
SIRTI drift at high count rate | Mean possible drift over all 18F measurements at the NIST. | B | 2 |
Ampoule dimensions | From the IRMM report [13] and sensitivity coefficients from Monte-Carlo simulations | B | 2* |
Ampoule filling height | Solution volume is 3.6(l) cm3; sensitivity coefficients from Monte-Carlo simulations | B | 2* |
Solution density | Between l g/cm3 and l.0l g/cm3 as requested in the protocol; sensitivity coefficients from Monte-Carlo simulations | B | 0.7 |
Measurement time | l s uncertainty | B | l |
Relative combined standard uncertainty | 3.9 |
Included in the type A uncertainty of the measurements of two ampoules of 18F