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. Author manuscript; available in PMC: 2020 Oct 22.
Published in final edited form as: Metrologia. 2017;54(1A):https://doi.org/10.1088/0026-1394/54/1a/06011.

Table 4a:

Uncertainty budgets for the SIRTI measurement of the 18F ampoules

Uncertainty contributions due to Comments Evaluation method Relative standard uncert. × 104
18F to 94Nb meas. ratio including live-time, background, decay corrections and threshold setting Standard uncertainty of the weighted mean of 33 measurements, taking into account the correlation due to the 18F half-life A 2.4
Long-term stability of the SIRTI Weighted standard deviation of 85 series, each series consisting of 10 measurements A 0.3
Nb-l bias from the mean since 2007 Relative difference from the mean B 1.8
Effect of decay on the live-time correction Maximum measurement duration evaluated from [12] B < l
SIRTI drift at high count rate Mean possible drift over all 18F measurements at the NIST. B 2
Ampoule dimensions From the IRMM report [13] and sensitivity coefficients from Monte-Carlo simulations B 2*
Ampoule filling height Solution volume is 3.6(l) cm3; sensitivity coefficients from Monte-Carlo simulations B 2*
Solution density Between l g/cm3 and l.0l g/cm3 as requested in the protocol; sensitivity coefficients from Monte-Carlo simulations B 0.7
Measurement time l s uncertainty B l
Relative combined standard uncertainty 3.9
*

Included in the type A uncertainty of the measurements of two ampoules of 18F