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(a) Chemical schematic for one-pot AB2 miktoarm star formation using a sequential deprotection–conjugation strategy between two-arm NBD-functionalized PLA (P6) and maleimide-terminated PnBMA (P7) to yield P8. Note: quenched with norbornene after 5 h. (b) SEC-RI overlay of polymer precursors and purified AB2 miktoarm star (P8). (c) SAXS data confirming self-assembly of P8 to a well-ordered lamellar structure.
