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. 2020 Jun 17;22(13):4970–4973. doi: 10.1021/acs.orglett.0c01471

Table 1. Optimizations of the CM Reaction of Sulfonamide 3a and Alkene 2a.

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entry solvent catalyst GC conversiona (%)
1 DCM 1a 76
2 DCM 1b 92
3 DCM 1c 89
4 toluene 1c 81
5 diethyl ether 1c 87
6 DCM 1d 57
a

Tetradecane was used as an internal standard.