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. 2020 Sep 29;12(10):2248. doi: 10.3390/polym12102248

Table 3.

Results of tensile tests made on plasticized flours and their blends with PCL and polybutylene adipate terephthalate (PBAT), by varying the biopolymer amounts, processing temperatures and mixing rate.

Sample Flour Glycerol (% wt.) Biopolymer (% wt.) Citric Acid (% wt.) Tset * Screw Speed (rpm) Ultimate Tensile Strength (MPa) Strain at Break (%)
TPF0 F0 23 0 0 2 30 1.23 ± 0.05 54.13 ± 4.39
TPF1 F1 23 0 0 2 30 2.63 ± 0.10 32.23 ± 0.64
TPF2 F2 23 0 0 2 30 2.62 ± 0.40 23.84 ± 2.45
TPF3 F3 23 0 0 2 30 3.83 ± 0.20 19.64 ± 1.60
TPF2_CA F2 23 0 0.8 2 30 1.61 ± 0,08 34.89 ± 2.44
TPF2_20BAT F2 23 20 PBAT 0 2 30 2.21 ± 0,17 6.93 ± 0.47
TPF2_20CL F2 23 20 PCL 0 2 30 1.96 ± 0.06 16.80 ± 1.98
TPF2_CA20BAT F2 23 20 PBAT 0.8 2 30 1.50 ± 0.05 10.44 ± 0.17
TPF2_CA20CL F2 23 20 PCL 0.8 2 30 1.66 ± 0.34 60.39 ± 13.00
F0_CA2 F0 17 0 0.8 2 30 1.54 ± 0.02 75.47 ± 11.66
F0_CA3 F0 17 0 0.8 3 30 1.05 ± 0.14 31.08 ± 6.07
F0_CA20CL2 F0 17 20 PCL 0.8 2 30 2.89 ± 0.23 61.80 ± 11,87
F0_CA20CL3 F0 17 20 PCL 0.8 3 30 2.69 ± 0.22 47.04 ± 18.15
F2_CA20CL2 F2 17 20 PCL 0.8 2 30 3,10 ± 0,24 12,42 ± 1,43
F2_CA20CL3 F2 17 20 PCL 0.8 3 30 2,72 ± 0,23 13,83 ± 1,12
F2_20CL F2 17 20 PCL 0.8 2 30 3.10 ± 0.24 12.42 ± 1.43
F2_20CL120R F2 17 20 PCL 0.8 2 120 3.17 ± 0.20 14.15 ± 2.46
F2_25CL F2 17 25 PCL 0.8 2 30 3.05 ± 0.03 16.27 ± 1.47
F2_25CL120R F2 17 25 PCL 0.8 2 120 3.70 ± 0.16 18.87 ± 2.77
F2_30CL F2 17 30 PCL 0.8 2 30 3.69 ± 0.43 12.49 ± 1.03
F2_30CL120R F2 17 30 PCL 0.8 2 120 3.43 ± 0.36 11.73 ± 0.99
F2_40CL F2 17 40 PCL 0.8 2 30 4,57 ± 0.36 30.75 ± 1.97
F2_40CL120R F2 17 40 PCL 0.8 2 120 4,63 ± 0.13 52.64 ± 4.02
F0_25CL120R F0 17 25 PCL 0.8 2 120 2.68 ± 0.11 57.11 ± 6.29
F1_25CL120R F1 17 25 PCL 0.8 2 120 3.58 ± 0.14 37.39 ± 4.07
F3_25CL120R F3 17 25 PCL 0.8 2 120 3.91 ± 0.31 10.04 ± 3.92

* Tset 2 = 130–135–140 °C; 3 = 135–140–145 °C.