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. 2020 Oct 30;10:18726. doi: 10.1038/s41598-020-72497-3

Table 2.

Myco-components detected in ethyl acetate total culture extract of C. globosum by GC–MS analysis.

S. no Name of the component Chemical formula Retention time (mins) Relative abundance (%)
1 Disiloxane, 1,3-bis(chloromethyl)-1,1,3,3-tetramethyl- C6H16Cl2OSi2 7.197 0.9299 ± 0.5
2 Carbamodithioic acid, phenyl-, methyl ester C8H9NS2 7.291 0.003015 ± 0.1
3 N-(Trimethylsilyl)acetamide CH3CONHSi (CH3)3 7.3048 0.5491 ± 0.8
4 2-Butenoic acid, tert-butyldimethylsilyl ester C17H36O3Si2 7.8719 0.15488 ± 0.1
5 Formamide, N,N-diethyl- HCON(C2H5)2 7.886 0.8218 ± 1.1
6 Isoquinolin-6,7-diol, 1-methyl C10H9NO2 8.2131 1.2960 ± 1.7
7 1-Hexene, 4,5-dimethyl- C8H16 8.2312 1.30402 ± 0.1
8 Sulfurous acid, di(cyclohexylmethyl) ester C14H26O3S 8.2767 0.01376 ± 0.1
9 Azetidine, 1-acetyl-2-methyl- C6H11NO 8.2854 2.83459 ± 0.2
10 Disilathiane, hexamethyl C6H18SSi2 8.348 1.39148 ± 0.1
11 2,4,4-Trimethyl-1-hexene C9H18 8.4016 0.4074 ± 0.6
12 Acetamide, N-ethyl- C4H9NO 8.8449 0.3275 ± 0.5
13 Tris(trimethylsilyl)borate C9H27BO3Si3 9.1013 0.557147 ± 0.1
14 1,2-Bis(trimethylsiloxy)ethane C8H22O2Si2 9.1285 0.8199 ± 1.1
15 Silanol, trimethyl-, carbonate (2:1) C7H18O3Si2 8.7307 0.3330 ± 0.5
16 Acetamide, N-ethyl- C4H9NO 8.8449 0.3280 ± 0.5
17 1,2-Bis(trimethylsiloxy)ethane C8H22O2Si2 9.1285 0.8200 ± 1.1
18 Acetamide, N,N-diethyl- C6H13NO 9.5024 1.5998 ± 2.2
19 2,2-Diethylacetamide C6H13NO 10.0863 2.5606 ± 3.6
20 Tris(trimethylsilyl)carbamate C10H27NO2Si3 10.316 0.1908 ± 0.3
21 N,N-Diethyl(trimethylsilyl)carbamate C8H19NO2Si 11.0868 0.2737 ± 0.4
22 Propanoic acid, 2-[(trimethylsilyl)oxy]-, trimethylsilyl ester C9H22O3Si2 11.2173 0.5037 ± 0.7
23 Acetic acid, [(trimethylsilyl)oxy]-, trimethylsilyl ester C8H20O3Si2 11.7152 1.2734 ± 1.8
24 Isophorone C9H14O 13.1412 0.3485 ± 0.5
25 Silanol, trimethyl-, phosphate (3:1) C9H27O4PSi3 17.332 0.4860 ± 0.7
26 Glycerol, tris(trimethylsilyl) ether C12H32O3Si3 17.4314 0.8582 ± 1.2
27 Butanedioic acid, bis(trimethylsilyl) ester C10H22O4Si2 18.5644 0.3425 ± 0.5
28 2-(2-Butoxyethoxy)ethoxy-trimethylsilane C11H26O3Si 19.1932 0.2287 ± 0.3
29 L-Proline, 5-oxo-1-(trimethylsilyl)-, trimethylsilyl ester C11H23NO3Si2 23.7834 0.2626 ± 0.4
30 Tricyclo[5.2.1.0(2,6)]decane, 3-methylene-4-phenyl C17H20 27.9234 1.3391 ± 1.9
31 1,4-Benzenedicarboxylic acid, bis(trimethylsilyl) ester C14H22O4Si2 29.9265 0.2885 ± 0.4
32 1-Nonadecene C19H38 30.1214 0.1761363 ± 0.2
33 Azelaic acid, bis(trimethylsilyl) ester C15H32O4Si2 30.1519 0.1670219 ± 0.8
34 D-(-)-Ribofuranose, tetrakis(trimethylsilyl) ether (isomer 2) C17H42O5Si4 31.0492 0.6179 ± 0.9
35 Salbutamol, N-trifluoroacetyl-O,O,o-tris(trimethylsilyl)deriv C24H44F3NO4Si3 31.309 0.3250 ± 0.5
36 α-D-Allopyranose, pentakis(trimethylsilyl) ether C21H52O6Si5 32.3191 0.2874 ± 0.4
37 Hexadecanoic acid, trimethylsilyl ester C19H40O2Si 35.1335 3.0713 ± 4.0
38 9,12-Octadecadienoic acid (Z,Z)-, trimethylsilyl ester C21H40O2Si 38.1093 3.3908 ± 4.7
39 Oleic acid, trimethylsilyl ester C21H42O2Si 38.2218 1.7593 ± 2.4
40 trans-9-Octadecenoic acid, trimethylsilyl ester C21H42O2Si 38.2268 7.27069 ± 0.8
41 Octadecanoic acid, trimethylsilyl ester C21H44O2Si 38.7029 3.2747 ± 4.6
42 Stearic acid, 2-(1-octadecenyloxy)ethyl ester, (Z)- C38H74O3 42.4672 1.2604 ± 1.8
43 Hexadecanoic acid, 2,3-bis[(trimethylsilyl)oxy]propyl ester C25H54O4Si2 44.2692 0.4854 ± 0.7
44 Chrysin, bis(trimethylsilyl) ether C21H26O4Si2 44.6518 12.8317 ± 3.5
45 Octadecanoic acid, 2,3-bis[(trimethylsilyl)oxy] propyl ester C27H58O4Si2 47.0836 2.1723 ± 3.0
46 .psi.,.psi.-Carotene, 1,1′,2,2′-tetrahydro-1,1′-dimethoxy- C42H64O2 52.9052 0.0880 ± 0.1

Chrysin (highlighted in bold) was one of the myco-components detected in the ethyl acetate total culture extract of C. globosum. The components were identified by comparing the spectrum of the unknown components with the spectrum of reported components in the National Institute Standard and Technology (NIST) library. The relative abundance of each component was calculated by comparing its average peak area to the total area contributed by all the components.